(1R,3aS,4S,8bR)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

Base Information Edit

Chemical Name:(1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate
CAS No.:138175-73-2
Molecular Formula:C₂₈H₄₀O₆S₂Si
Molecular Weight:564.839
Hs Code.:
Mol file:138175-73-2.mol

(1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

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Suppliers and Price of (1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

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Chemical Property of (1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate Edit

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Technology Process of (1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

There total 32 articles about (1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-2-{1-[2-(2,2-Dimethoxy-ethyl)-[1,3]dithian-2-yl]-2-[2-methylene-dihydro-furan-(3E)-ylidene]-ethoxymethyl}-3-(dimethyl-phenyl-silanyl)-acrylic acid methyl ester

: 138175-73-2,138285-32-2
(1R*,3aR*,4R*,*8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

: 138175-73-2,138285-32-2
(1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

Guidance literature:: With N-ethyl-diisopropylethylamine; hydroquinone; In toluene; at 85 ℃; for 4h; Yield given. Yields of byproduct given;
DOI:10.1039/P19920002735

Reference yield:

: (E)-2-{1-[2-(2,2-Dimethoxy-ethyl)-[1,3]dithian-2-yl]-2-[2-methylene-dihydro-furan-(3E)-ylidene]-ethoxymethyl}-3-(dimethyl-phenyl-silanyl)-acrylic acid methyl ester

: 138175-73-2,138285-32-2
(1R*,3aR*,4R*,*8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

: 138175-73-2,138285-32-2
(1R*,3aS*,4S*,8bR*)-methyl 1-<2'-(2'',2''-dimethoxyethyl)-1',3'-dithian-2'-yl>-4-dimethyl(phenyl)silyl-1,4,5,7,8,8b-hexahydro-3H-benzo<1,2-b:3,4-c'>difuran-3a-carboxylate

Guidance literature:: With N-ethyl-diisopropylethylamine; hydroquinone; In toluene; at 85 ℃; for 4h; Yield given. Yields of byproduct given;
DOI:10.1039/P19920002735