((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester

Base Information

Chemical Name:((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester
CAS No.:132149-84-9
Molecular Formula:C₁₇H₂₇NO₂S
Molecular Weight:309.473
Hs Code.:

Synonyms:

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Chemical Property of ((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester

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Technology Process of ((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester

There total 11 articles about ((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 132149-84-9
((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, DMAP / CH₂Cl₂

2: H₂ / Pd/C / acetic acid

3: n-Bu₃P / tetrahydrofuran

With dmap; tributylphosphine; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid;

Reference yield:

: (2S,3S)-2-Methoxymethoxy-3-methyl-pentan-1-ol

: 132149-84-9
((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) NaH / 1.) DMF

2: aq. HCl / tetrahydrofuran

3: Et₃N / CH₂Cl₂

4: NaN₃ / dimethylformamide / 90 °C

5: LiAlH₄ / tetrahydrofuran

6: Et₃N, DMAP / CH₂Cl₂

7: H₂ / Pd/C / acetic acid

8: n-Bu₃P / tetrahydrofuran

With hydrogenchloride; dmap; lithium aluminium tetrahydride; sodium azide; tributylphosphine; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 56577-28-7
methyl (2S,3S)-2-hydroxy-3-methylpentanoate

: 132149-84-9
((1R,2S)-2-Methyl-1-phenylsulfanylmethyl-butyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: i-PrNEt₂ / CH₂Cl₂

2: LiAlH₄ / tetrahydrofuran

3: 1.) NaH / 1.) DMF

4: aq. HCl / tetrahydrofuran

5: Et₃N / CH₂Cl₂

6: NaN₃ / dimethylformamide / 90 °C

7: LiAlH₄ / tetrahydrofuran

8: Et₃N, DMAP / CH₂Cl₂

9: H₂ / Pd/C / acetic acid

10: n-Bu₃P / tetrahydrofuran

With hydrogenchloride; dmap; lithium aluminium tetrahydride; sodium azide; N,N-diethyl-N-isopropylamine; tributylphosphine; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide;