{Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}(B(C₆H₅)4)2

Base Information

• Chemical Name: {Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}(B(C₆H₅)4)2
• CAS No.: 111140-32-0
• Molecular Formula: 2C₂₄H₂₀B*C₂₈H₃₄CoN₆
• Molecular Weight: 1152.08

Synonyms:

Chemical Property of {Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}(B(C₆H₅)4)2

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Technology Process of {Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}(B(C₆H₅)4)2

There total 1 articles about {Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}(B(C₆H₅)4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(3+)*3ClO4(1-)={Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(ClO4)3 (103093-30-7) + sodium tetraphenyl borate (143-66-8) + acetonitrile (75-05-8,26809-02-9) → {Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(2+)*2B(C6H5)4(1-)={Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(B(C6H5)4)2 (111140-32-0)

Guidance literature:

In ethanol; acetonitrile; slurrying with acetonitrile/ethanol (1:1); refluxing slurry until solid dissolves (10 h); filtration and addn. of NaB(C6H5)4 (2 mol/mol of Co) to filtrate;; crystn.; recrystn. from acetonitrile in inert-atmosphere glovebox; elem. anal.; detn. by electronic absorption, IR and ESR;;

DOI:10.1021/ic00272a011

Reference yield:

{Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(2+)*2B(C6H5)4(1-)={Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(B(C6H5)4)2 (111140-32-0) → {Co(C10H12N4(CH3)2(C6H5)2)}(1+) (111140-38-6)

Guidance literature:

In water; Electrolysis; controlled-potential electrolysis at -0.50 V (0.1 M (C4H9)4NClO4, aq. SCE) until current falls to 1% of initial value (inert-atmosphere glovebox);; not isolated from soln., characterization by electronic absorption spectroscopy, ESR and cyclic voltammetry;;

DOI:10.1021/ic00272a011

Reference yield:

pyridine (110-86-1) + {Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(2+)*2B(C6H5)4(1-)={Co(C10H12N4(CH3)2(C6H5)2)(CH3CN)2}(B(C6H5)4)2 (111140-32-0) → {Co(C10H12N4(CH3)2(C6H5)2)(NC5H5)}(1+)

Guidance literature:

In acetonitrile; addn. of slight stoich. excess of pyridine to soln. in acetonitrile;; not isolated from soln., detected by electronic spectrum;;

DOI:10.1021/ic00272a011

upstream raw materials:

{Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}⁽³⁺⁾*3ClO₄^(1-)={Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)(CH₃CN)2}(ClO₄)3

sodium tetraphenyl borate

acetonitrile

Downstream raw materials:

{Co(C₁₀H₁₂N₄(CH₃)2(C₆H₅)2)}⁽¹⁺⁾

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