Piv-Proψα(N^βHZ)>Gly-NHiPr

Base Information

Chemical Name:Piv-Proψα(N^βHZ)>Gly-NHiPr
CAS No.:135904-48-2
Molecular Formula:C₂₃H₃₄N₄O₅
Molecular Weight:446.547
Hs Code.:

Piv-Proψ<CO-N<sup>α</sup>(N<sup>β</sup>HZ)>Gly-NHiPr

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Piv-Proψα(N^βHZ)>Gly-NHiPr

Chemical Property:

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Technology Process of Piv-Proψα(N^βHZ)>Gly-NHiPr

There total 8 articles about Piv-Proψα(N^βHZ)>Gly-NHiPr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {N'-Benzyloxycarbonyl-N-[(S)-1-(2,2-dimethyl-propionyl)-pyrrolidine-2-carbonyl]-hydrazino}-acetic acid

: 75-31-0
isopropylamine

: 135904-48-2
Piv-Proψα(N^βHZ)>Gly-NHiPr

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃;
DOI:10.1016/0040-4039(91)85080-O

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 135904-48-2
Piv-Proψα(N^βHZ)>Gly-NHiPr

Guidance literature:: Multi-step reaction with 6 steps

1: NMM / tetrahydrofuran / 0 °C

2: NMM / CH₂Cl₂ / -10 °C

3: 3N HCl / ethyl acetate

4: NaHCO₃ / CH₂Cl₂ / 0 °C

5: 1N aq. NaOH / acetone / 0 °C

6: i-BuOCOCl, NMM / tetrahydrofuran / -15 °C

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone;
DOI:10.1016/0040-4039(91)85080-O

Reference yield:

: 4503-58-6
benzyl 2-(2-ethoxy-2-ethoxyethyl)-1-hydrazinecarboxylate

: 135904-48-2
Piv-Proψα(N^βHZ)>Gly-NHiPr

Guidance literature:: Multi-step reaction with 5 steps

1: NMM / CH₂Cl₂ / -10 °C

2: 3N HCl / ethyl acetate

3: NaHCO₃ / CH₂Cl₂ / 0 °C

4: 1N aq. NaOH / acetone / 0 °C

5: i-BuOCOCl, NMM / tetrahydrofuran / -15 °C

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone;
DOI:10.1016/0040-4039(91)85080-O