MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂⁽¹⁺⁾*Br^(1-)={MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂}Br

Base Information

Chemical Name:MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂⁽¹⁺⁾*Br^(1-)={MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂}Br
CAS No.:108557-97-7
Molecular Formula:Br*C₃₇H₃₀BrMoN₂O₂P₂
Molecular Weight:852.353
Hs Code.:

MoBr(CO)2(C<sub>5</sub>H<sub>4</sub>N)2(C<sub>6</sub>H<sub>5</sub>)4P<sub>2</sub>CH<sub>2</sub><sup>(1+)</sup>*Br<sup>(1-)</sup>={MoBr(CO)2(C<sub>5</sub>H<sub>4</sub>N)2(C<sub>6</sub>H<sub>5</sub>)4P<sub>2</sub>CH<sub>2</sub>}Br

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Chemical Property of MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂⁽¹⁺⁾*Br^(1-)={MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂}Br

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Technology Process of MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂⁽¹⁺⁾*Br^(1-)={MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂}Br

There total 3 articles about MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂⁽¹⁺⁾*Br^(1-)={MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂}Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 15668-64-1
tetracarbonyl(2,2'-bipyridine)molybdenum

: 2071-20-7
bis-diphenylphosphinomethane

: 108557-97-7
MoBr₂(CO)2(2,2'-bipyridine)(bis(diphenylphosphino)methane)

Guidance literature:: With bromine; In tetrachloromethane; dichloromethane; To a soln. of complex in CH2Cl2 was added a soln. of Br2 in CCl4 under N2 atm., mixt. was stirred; dppm was added and mixt. was stirred for 30 min in the absence of light at room temp.;; evapd., hexane was added, ppt. was washed with Et2O, recrystd. from CH2Cl2-hexane; elem. anal.;;

Reference yield:

: 108581-58-4
2,2'-bipyridine{bis(diphenylphosphino)methane}dibromo(carbonyl)molybdenum(II)

: 108557-97-7
MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂⁽¹⁺⁾*Br^(1-)={MoBr(CO)2(C₅H₄N)2(C₆H₅)4P₂CH₂}Br

Guidance literature:: With CO; In dichloromethane; CO (1 atm.); not sepd.; detected by IR spectra;;

Reference yield:

: 15668-64-1
tetracarbonyl(2,2'-bipyridine)molybdenum

: 7726-95-6
bromine

: 2071-20-7
bis-diphenylphosphinomethane

: 108557-97-7
MoBr₂(CO)2(2,2'-bipyridine)(bis(diphenylphosphino)methane)

Guidance literature:: In tetrachloromethane; dichloromethane; Br2 added to the Mo carbonyl complex in CH2Cl2 at room temp. until formation of MoBr2(CO)3(bipy) is completed; dppm added to the reaction mixt.; concn., addn. of hexane affords the solid; washing with Et2O, recrystn. from CH2Cl2-hexane;
DOI:10.1016/S0020-1693(00)86376-8