Ac-Ala₃-PheCH₃

Base Information

Chemical Name:Ac-Ala₃-PheCH₃
CAS No.:90427-67-1
Molecular Formula:C₂₁H₃₀N₄O₅
Molecular Weight:418.493
Hs Code.:

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Chemical Property of Ac-Ala₃-PheCH₃

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Technology Process of Ac-Ala₃-PheCH₃

There total 5 articles about Ac-Ala₃-PheCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-24-7
acetic anhydride

: 90427-76-2
Ala₃-PheCH₃, HBr

: 90427-67-1
Ac-Ala₃-PheCH₃

Guidance literature:: In pyridine; for 2h; Ambient temperature;

Reference yield:

: 111491-96-4
(S)-3-(N-(benzyloxycarbonyl)amino)-4-phenyl-2-butanone

: 90427-67-1
Ac-Ala₃-PheCH₃

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, 2 N HCl / Pd

2: 98 percent / NEt₃, ethyl chlorocarbonate / dimethylformamide; tetrahydrofuran

3: HBr / acetic acid

4: 60 percent / pyridine / 2 h / Ambient temperature

With hydrogenchloride; hydrogen bromide; hydrogen; chloroformic acid ethyl ester; triethylamine; palladium; In tetrahydrofuran; pyridine; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 13585-98-3
N^α-benzyloxycarbobyl-L-alanyl-L-alanyl-L-alanine

: 90427-67-1
Ac-Ala₃-PheCH₃

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NEt₃, ethyl chlorocarbonate / dimethylformamide; tetrahydrofuran

2: HBr / acetic acid

3: 60 percent / pyridine / 2 h / Ambient temperature

With hydrogen bromide; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; pyridine; acetic acid; N,N-dimethyl-formamide;