C₁₃H₁₄N₂O₂

Base Information

Chemical Name:C₁₃H₁₄N₂O₂
CAS No.:130872-74-1
Molecular Formula:C₁₃H₁₄N₂O₂
Molecular Weight:230.266
Hs Code.:

C<sub>13</sub>H<sub>14</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₄N₂O₂

Chemical Property:

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Technology Process of C₁₃H₁₄N₂O₂

There total 5 articles about C₁₃H₁₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54308-43-9
2-(3-methoxyphenyl)-1,3-dithiane

: 130872-74-1
C₁₃H₁₄N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi, TMEDA / 1.) 2-methyl-THF, r.t.; 2.) 2-methyl-THF, -100 deg C to r.t.

2: 78 percent / NaH / tetrahydrofuran / Heating

3: 40 percent / Raney Ni / ethanol / Heating

4: 59 percent / EtSH, BF₃*Et₂O / Ambient temperature

5: 2.) Amberlite IRA-400 (OH-) / 1.) EtOH, reflux; 2.) MeOH, r.t.

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; Amberlite IRA-400 (OH-); boron trifluoride diethyl etherate; nickel; sodium hydride; ethanethiol; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4039(00)97732-3

Reference yield:

: 130872-75-2
2-Chloro-6-[2-(3-methoxy-phenyl)-[1,3]dithian-2-yl]-pyrazine

: 130872-74-1
C₁₃H₁₄N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / NaH / tetrahydrofuran / Heating

2: 40 percent / Raney Ni / ethanol / Heating

3: 59 percent / EtSH, BF₃*Et₂O / Ambient temperature

4: 2.) Amberlite IRA-400 (OH-) / 1.) EtOH, reflux; 2.) MeOH, r.t.

With Amberlite IRA-400 (OH-); boron trifluoride diethyl etherate; nickel; sodium hydride; ethanethiol; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4039(00)97732-3

Reference yield:

: 2-Benzyloxy-6-[2-(3-methoxy-phenyl)-[1,3]dithian-2-yl]-pyrazine

: 130872-74-1
C₁₃H₁₄N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / Raney Ni / ethanol / Heating

2: 59 percent / EtSH, BF₃*Et₂O / Ambient temperature

3: 2.) Amberlite IRA-400 (OH-) / 1.) EtOH, reflux; 2.) MeOH, r.t.

With Amberlite IRA-400 (OH-); boron trifluoride diethyl etherate; nickel; ethanethiol; In ethanol;
DOI:10.1016/S0040-4039(00)97732-3