4'-(3-2)>propylamino)acetophenon

Base Information

• Chemical Name: 4'-(3-2)>propylamino)acetophenon
• CAS No.: 75501-86-9
• Molecular Formula: C₂₁H₂₈N₆O₁₁P₂
• Molecular Weight: 602.434
• Mol file: 75501-86-9.mol

Synonyms:

Chemical Property of 4'-(3-2)>propylamino)acetophenon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4'-(3-2)>propylamino)acetophenon

There total 3 articles about 4'-(3-2)>propylamino)acetophenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-(3-Hydroxypropylamino)acetophenon (75501-87-0) → 4'-(3-2)>propylamino)acetophenon (75501-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / 1) metaphosphoric acid, 2) Dowex (H+) / H₂O / 4 h / 80 °C

2: various solvent(s) / 168 h / 22 °C

With Dowex (H+); meta-phosphoric acid; In water;

Reference yield:

p-aminobenzophenone (99-92-3) → 4'-(3-2)>propylamino)acetophenon (75501-86-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 18 percent / NaI / ethanol / 75 h / Heating

2: 46 percent / 1) metaphosphoric acid, 2) Dowex (H+) / H₂O / 4 h / 80 °C

3: various solvent(s) / 168 h / 22 °C

With Dowex (H+); meta-phosphoric acid; sodium iodide; In ethanol; water;

Reference yield:

3-(4'-Acetylanilino)propylhydrogenphosphat (75501-88-1) + adenosine 5'-monophosphate morpholidate (7331-13-7) → 4'-(3-2)>propylamino)acetophenon (75501-86-9)

Guidance literature:

In various solvent(s); at 22 ℃; for 168h; Yield given;

upstream raw materials:

3-(4'-Acetylanilino)propylhydrogenphosphat

adenosine 5'-monophosphate morpholidate

4'-(3-Hydroxypropylamino)acetophenon

p-aminobenzophenone