(2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one

Base Information

• Chemical Name: (2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one
• CAS No.: 199915-50-9
• Molecular Formula: C₂₆H₂₈N₄O₆
• Molecular Weight: 492.532

Synonyms:

Chemical Property of (2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one

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Technology Process of (2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one

There total 2 articles about (2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1-((2R,3R,4S,5S)-5-Dimethoxymethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-6-(1,3-diphenyl-imidazolidin-2-yl)-1H-pyrimidine-2,4-dione → (2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one (199915-50-9) + Carbonic acid (2S,3S,4R,5R)-2-dimethoxymethyl-5-[6-(1,3-diphenyl-imidazolidin-2-yl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-hydroxy-tetrahydro-furan-3-yl ester phenyl ester

Guidance literature:

With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide;

DOI:10.1080/07328319708006196

Reference yield: 31.0%

bis(phenyl) carbonate (102-09-0) + 1-((2R,3R,4S,5S)-5-Dimethoxymethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-6-(1,3-diphenyl-imidazolidin-2-yl)-1H-pyrimidine-2,4-dione → (2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one (199915-50-9) + Carbonic acid (2S,3S,4R,5R)-2-dimethoxymethyl-5-[6-(1,3-diphenyl-imidazolidin-2-yl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-4-hydroxy-tetrahydro-furan-3-yl ester phenyl ester

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide;

DOI:10.1080/07328319708006196

Reference yield:

(2S,3S,3aS,9aR)-2-Dimethoxymethyl-8-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one (199915-50-9) → (2S,3S,3aS,4aS,9aR)-2-Dimethoxymethyl-4a-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-hexahydro-furo[2',3':4,5]oxazolo[3,2-c]pyrimidine-6,8-dione (311815-38-0)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water;

DOI:10.1080/07328319708006196

upstream raw materials:

bis(phenyl) carbonate

Downstream raw materials:

(2S,3S,3aS,4aS,9aR)-2-Dimethoxymethyl-4a-(1,3-diphenyl-imidazolidin-2-yl)-3-hydroxy-hexahydro-furo[2',3':4,5]oxazolo[3,2-c]pyrimidine-6,8-dione

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