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102-09-0

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Cas No: 102-09-0
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Diphenyl carbonate
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USD $ 100.0-100.0 / Kilogram 1 Kilogram 100 Metric Ton/Month Xi'an Julong Bio-Tech Co., Ltd. Contact Supplier
Diphenyl carbonate
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DPC 99.5% cas 102-09-0 Pesticide Intermediates CAS No.: 102-09-0
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102-09-0 Diphenyl carbonate
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USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
102-09-0, factory price 99% Diphenyl carbonate from China supplier
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USD $ 3.0-5.0 / Gram 100 Gram 1000 Metric Ton/Month WUHAN MULEI NEW MATERIAL CO., LTD Contact Supplier

102-09-0 Usage

Chemical Properties

white solid

Definition

ChEBI: A carbonate ester that is the diphenyl ester of carbonic acid.

Safety Profile

Questionable carcinogen with experimental neoplastigenic and tumorigenic data. When heated to decomposition it emits acrid smoke and irritating fumes

Uses

In the molten state as solvent for nitrocellulose.
InChI:InChI=1/C13H10O3/c14-13(15-11-7-3-1-4-8-11)16-12-9-5-2-6-10-12/h1-10H

102-09-0 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A12362)  Diphenyl carbonate, 99%    102-09-0 250g 342.0CNY Detail
Alfa Aesar (A12362)  Diphenyl carbonate, 99%    102-09-0 1000g 792.0CNY Detail
Alfa Aesar (A12362)  Diphenyl carbonate, 99%    102-09-0 5000g 3365.0CNY Detail
Aldrich (D206539)  Diphenylcarbonate  ReagentPlus®, 99% 102-09-0 D206539-100G 338.13CNY Detail
Aldrich (D206539)  Diphenylcarbonate  ReagentPlus®, 99% 102-09-0 D206539-1KG 840.06CNY Detail
Vetec (V900532)  Diphenylcarbonate  Vetec reagent grade, 98% 102-09-0 V900532-500G 235.17CNY Detail

102-09-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name diphenyl carbonate

1.2 Other means of identification

Product number -
Other names phenyl phenoxyformate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:102-09-0 SDS

102-09-0Synthetic route

chloroform
67-66-3

chloroform

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With oxygen; sodium hydrogencarbonate; triethylamine In water for 1.5h; Irradiation;99%
With pyridine; oxygen at 20℃; for 1h; Time; Reagent/catalyst; Irradiation;99%
tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

phenyl chloroformate
1885-14-9

phenyl chloroformate

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
98%
methyl phenyl carbonate
13509-27-8

methyl phenyl carbonate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

phenyl chloroformate
1885-14-9

phenyl chloroformate

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
98%
3,3'-carbonylbis<5-phenyl-1,3,4-oxadiazole-2(3H)-thione>
122350-19-0

3,3'-carbonylbis<5-phenyl-1,3,4-oxadiazole-2(3H)-thione>

phenol
108-95-2

phenol

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

5-phenyl-1,3,4-oxadiazole-2(3H)-thione
3004-42-0

5-phenyl-1,3,4-oxadiazole-2(3H)-thione

Conditions
ConditionsYield
With pyridine In various solvent(s) for 192h; Ambient temperature;A 97%
B n/a
4-chloro-4'-fluorobutyrophenone-2,2-dimethylpropylene ketal

4-chloro-4'-fluorobutyrophenone-2,2-dimethylpropylene ketal

3-tert-butylphenyol
585-34-2

3-tert-butylphenyol

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

4-Fluoro-α-[3-(2-methyl-2-propyl)phenoxy]propylbenzenemethanol

4-Fluoro-α-[3-(2-methyl-2-propyl)phenoxy]propylbenzenemethanol

Conditions
ConditionsYield
With hydrogenchloride In methanol; N,N-dimethyl-formamideA 97%
B n/a
carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

phenol
108-95-2

phenol

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

methanol
67-56-1

methanol

Conditions
ConditionsYield
lead (II) phenoxide at 210 - 235℃; under 150.015 - 6750.68 Torr; for 500 - 6000h; Product distribution / selectivity; Heating / reflux;A 97%
B n/a
triphenylmethyl alcohol
76-84-6

triphenylmethyl alcohol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With trifluoroacetyl peroxide; trifluoroacetic acid In 1,1,2-Trichloro-1,2,2-trifluoroethane at -25℃; for 1h; Criegee rearrangement;96%
benzophenone diphenyl ketal
59550-02-6

benzophenone diphenyl ketal

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With trifluoroacetyl peroxide; trifluoroacetic acid In trichlorofluoromethane at -24℃; for 1h; Criegee rearrangement;96%
N,N′-hexanediyl bis-carbamic acid diphenyl ester
4223-31-8

N,N′-hexanediyl bis-carbamic acid diphenyl ester

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

Hexamethylene diisocyanate
822-06-0

Hexamethylene diisocyanate

Conditions
ConditionsYield
at 150℃; under 11.2511 - 112.511 Torr;A n/a
B 95.3%
tetraphenyl phosphonium chloride
2001-45-8

tetraphenyl phosphonium chloride

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With hydrogenchloride95.2%
With hydrogenchloride95.2%
With hydrogenchloride95.2%
carbon monoxide
201230-82-2

carbon monoxide

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With tetrabutylammomium bromide; oxygen at 65℃; under 36003.6 Torr; for 4h; Catalytic behavior; Reagent/catalyst; Autoclave;95%
With oxygen; tetrabutyl phosphonium bromide; p-benzoquinone; palladium diacetate; cerium(III) acetate In 1,2-propylene cyclic carbonate at 25 - 100℃; under 45004.5 - 47254.7 Torr; for 3h; Product distribution / selectivity;70%
With oxygen; tetrabutyl phosphonium bromide; p-benzoquinone; palladium diacetate; cerium(III) acetate In 1,2-propylene cyclic carbonate at 25 - 100℃; under 45004.5 - 47254.7 Torr; for 3h; Product distribution / selectivity;55%
diphenylthiocarbonate
13509-34-7

diphenylthiocarbonate

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With dinitrogen tetraoxide In tetrachloromethane; acetonitrile at 0℃; for 12h;94%
With hydrogenchloride; N-nitrosopiperidine; potassium iodide In hydrogenchloride; dichloromethane; water at 22℃; for 43h;78%
With hydrogenchloride; sodium nitrite In dichloromethane; water at 45℃; for 20h;15 % Chromat.
phenyl 4,5-dichloro-6-oxopyridazine-1(6H)-carboxylate
1202680-24-7

phenyl 4,5-dichloro-6-oxopyridazine-1(6H)-carboxylate

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With aluminum (III) chloride In toluene at 20℃; for 0.25h;94%
With potassium tert-butylate In toluene at 20℃; for 0.25h; Green chemistry;80%
tetrakis(triphenylphosphine) palladium(0)
14221-01-3

tetrakis(triphenylphosphine) palladium(0)

Phenyl cyanoformate
5532-82-1

Phenyl cyanoformate

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

trans-dicyanobis(triphenylphosphine)palladium(II)

trans-dicyanobis(triphenylphosphine)palladium(II)

Conditions
ConditionsYield
In toluene byproducts: CO; under Ar; NCCOOPh added to toluene dispersion of Pd(PPh3)4 at room temp.; stirred for 48 h; filtered; solid washed with hexane; dried under vac.; detd. by (1)H and (31)P NMR spectra;A 92%
B 83%
phenyl chloroformate
1885-14-9

phenyl chloroformate

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With pyridine In dichloromethane Condensation;90%
In pyridine; dichloromethane90%
N,N,N',N'-tetramethylchlorformamidinium chloride at 86.9℃; for 24h;
carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With 1H-imidazole; potassium carbonate at 95℃; under 750.075 Torr; for 9h; Time; Inert atmosphere;90%
With di(n-butyl)tin oxide at 180 - 200℃; for 12h; Inert atmosphere;18.6%
methyl phenyl carbonate
13509-27-8

methyl phenyl carbonate

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With titanium(IV) isopropylate at 180℃; for 3h; Catalytic behavior; Reagent/catalyst; Temperature; Inert atmosphere; Green chemistry;90%
at 160℃; under 375.038 Torr; for 3h; Temperature;81.9%
With N,N,N-triethyl-N-butanesulfonic acid ammonium hydrogen sulfate at 160℃; under 375.038 Torr; for 3h; Reagent/catalyst; Temperature; Pressure; Ionic liquid;81.9%
phosgene
75-44-5

phosgene

phenol
108-95-2

phenol

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

hydrogenchloride
7647-01-0

hydrogenchloride

Conditions
ConditionsYield
Stage #1: phenol; pyridine at 50 - 150℃; Heating / reflux;
Stage #2: phosgene at 150℃;
A 89.9%
B n/a
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With triethylamine In acetonitrile at 20℃; for 72h; Reagent/catalyst; Sealed tube;88%
phenylmagnesium bromide

phenylmagnesium bromide

phenyl chloroformate
1885-14-9

phenyl chloroformate

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

benzoic acid phenyl ester
93-99-2

benzoic acid phenyl ester

Conditions
ConditionsYield
With copper(I) bromide; lithium bromide In tetrahydrofuran at 20℃;A n/a
B 84%
phenyl fluoroformate
351-80-4

phenyl fluoroformate

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

fluorobenzene
462-06-6

fluorobenzene

Conditions
ConditionsYield
Pt/Al2O3 at 300℃;A 15%
B 80%
aluminum oxide In toluene at 400℃;A 40%
B 5%
phenyl chloroformate
1885-14-9

phenyl chloroformate

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With disodium telluride; tetrabutylammomium bromide In water; benzene for 0.25h; Ambient temperature;77%
With aluminum (III) chloride; butan-1-ol In toluene Reagent/catalyst; Temperature; Reflux;20%
With diethyl ether; magnesium ethylate
phenylpropiolic acid sodium salt
7063-23-2

phenylpropiolic acid sodium salt

phenyl chloroformate
1885-14-9

phenyl chloroformate

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

phenyl 3-phenyl-2-propynoate
100954-03-8

phenyl 3-phenyl-2-propynoate

C

4-phenylnaphtho[2,3-c]furan-1,3-dione
1985-37-1

4-phenylnaphtho[2,3-c]furan-1,3-dione

Conditions
ConditionsYield
In tetrahydrofuran at 40 - 67℃;A n/a
B n/a
C 73%
methyl phenyl carbonate
13509-27-8

methyl phenyl carbonate

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

Conditions
ConditionsYield
With SiO2 supported 15 wt% MoO3 at 200℃; for 2h; Kinetics; Reagent/catalyst; Inert atmosphere;A 71.4%
B n/a
catalyst C at 195℃; under 225.023 Torr; Product distribution / selectivity;
titanium(IV) phenoxide at 195℃; under 225.023 Torr; Product distribution / selectivity;
2-chlorocarbonyloxy-1,1,1,3,3,3-hexafluoro-2-trifluoromethyl-propane
27746-96-9

2-chlorocarbonyloxy-1,1,1,3,3,3-hexafluoro-2-trifluoromethyl-propane

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With triethylamine In diethyl ether for 24h;70%
sodium propargylate
920-38-7

sodium propargylate

phenyl chloroformate
1885-14-9

phenyl chloroformate

A

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

B

phenyl prop-2-ynoate
60998-71-2

phenyl prop-2-ynoate

Conditions
ConditionsYield
In tetrahydrofuran at 25 - 40℃; for 2h; Substitution;A n/a
B 70%
urea
57-13-6

urea

phenol
108-95-2

phenol

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
With iron(III) nitrate hexahydrate; nitric acid In tetrahydrofuran at 70℃;70%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

A

sodium phenoxide
139-02-6

sodium phenoxide

B

sodium salicylat
81256-74-8

sodium salicylat

Conditions
ConditionsYield
With water; sodium hydroxide In dimethyl sulfoxide at 25℃; Kinetics;A 100%
B n/a
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

4,4'-diamino diphenyl methane
101-77-9

4,4'-diamino diphenyl methane

4,4'-methylenediphenylene biscarbamate

4,4'-methylenediphenylene biscarbamate

Conditions
ConditionsYield
With 4-nitro-benzoic acid In toluene at 80℃; for 16h; Reagent/catalyst; Inert atmosphere;100%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

uridine
58-96-8

uridine

2,2'-Anhydrouridine
3736-77-4

2,2'-Anhydrouridine

Conditions
ConditionsYield
Stage #1: bis(phenyl) carbonate; uridine In N,N-dimethyl-formamide at 80℃; for 1h; Inert atmosphere;
Stage #2: With sodium hydrogencarbonate at 115℃; for 4h;
100%
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 100℃; for 4h; Inert atmosphere;
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

6-aminohexanoic acid
60-32-2

6-aminohexanoic acid

1,3-bis(5-carboxypentyl)urea
6630-04-2

1,3-bis(5-carboxypentyl)urea

Conditions
ConditionsYield
With triethylamine In dimethyl sulfoxide for 4.5h; Reflux;100%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

1,6-Hexanediamine
124-09-4

1,6-Hexanediamine

N,N′-hexanediyl bis-carbamic acid diphenyl ester
4223-31-8

N,N′-hexanediyl bis-carbamic acid diphenyl ester

Conditions
ConditionsYield
With lead(II) oxide In phenol at 50℃; Product distribution / selectivity; Industry scale;99.5%
With phenol at 50℃; Product distribution / selectivity; Industry scale;99.5%
With phenol at 50℃; Industrial scale;99.5%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

3-aminomethyl-3,5,5-trimethylcyclohexylamine
2855-13-2

3-aminomethyl-3,5,5-trimethylcyclohexylamine

3-(phenoxycarbonylamino-methyl)-3,5,5-trimethylcyclohexyl carbamic acid phenyl ester
126249-14-7

3-(phenoxycarbonylamino-methyl)-3,5,5-trimethylcyclohexyl carbamic acid phenyl ester

Conditions
ConditionsYield
With lead(II) oxide In phenol at 50℃; Product distribution / selectivity; Industry scale;99.3%
lead(II) oxide In phenol at 50℃; Industry scale;99.3%
With phenol at 50℃; Product distribution / selectivity; Industry scale;99.3%
In phenol at 50℃;99.3%
In phenol93%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

4,4'-diaminodicyclohexylmethane
1761-71-3

4,4'-diaminodicyclohexylmethane

phenyl N-[4-({4-[(phenoxycarbonyl)amino]cyclohexyl}methyl)cyclohexyl]carbamate
439680-99-6

phenyl N-[4-({4-[(phenoxycarbonyl)amino]cyclohexyl}methyl)cyclohexyl]carbamate

Conditions
ConditionsYield
With iron(II) diacetylacetonate In phenol at 50℃; Product distribution / selectivity; Industry scale;99.1%
With phenol; ferrous acetylacetonate at 50℃; Product distribution / selectivity; Industry scale;99.2%
With iron(II) acetylacetonate In phenol at 50℃; Reagent/catalyst;99.1%
In phenol Large scale;95%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

phenol
108-95-2

phenol

Conditions
ConditionsYield
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate; hydrogen In tetrahydrofuran at 140℃; under 38002.6 Torr; for 10h; Autoclave;99%
With calcium carbide; caesium carbonate In water; dimethyl sulfoxide at 140℃; for 16h; Inert atmosphere; Green chemistry;74%
With potassium tert-butylate; hydrogen; C16H18BrCoINO2 In dibutyl ether at 160℃; under 45004.5 Torr; for 20h; Sealed tube; Autoclave;64%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

1,6-Hexanediamine
124-09-4

1,6-Hexanediamine

phenol
108-95-2

phenol

N,N′-hexanediyl bis-carbamic acid diphenyl ester
4223-31-8

N,N′-hexanediyl bis-carbamic acid diphenyl ester

Conditions
ConditionsYield
at 45 - 60℃; for 1.33333h; Product distribution / selectivity;99%
at 50 - 60℃; for 1.33333h; Product distribution / selectivity;
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

indole
120-72-9

indole

phenyl 1H-indole-1-carboxylate
74117-31-0

phenyl 1H-indole-1-carboxylate

Conditions
ConditionsYield
With sodium carbonate In acetonitrile at 20 - 120℃; for 24h; Reagent/catalyst; Solvent; Temperature; Schlenk technique; regioselective reaction;99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene at 59.84℃; for 3h;76%
With 1,8-diazabicyclo[5.4.0]undec-7-ene
With 1,8-diazabicyclo[5.4.0]undec-7-ene In neat (no solvent) at 59.84℃; for 3h; Temperature; Time; Concentration; Inert atmosphere; Green chemistry; regioselective reaction;
With polystyrene-supported 1,8-diazabicyclo[5.4.0]-undec-7-ene In neat (no solvent) at 159.84℃; for 4h; Temperature; Time; Inert atmosphere; Schlenk technique;
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

phenylethane 1,2-diol
93-56-1

phenylethane 1,2-diol

4-Phenyl-1,3-dioxolan-2-one
4427-92-3

4-Phenyl-1,3-dioxolan-2-one

Conditions
ConditionsYield
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In 2-methyltetrahydrofuran at 30℃; for 2h; Reagent/catalyst; Solvent;99%
With iron(II) bromide In 1,4-dioxane at 150℃; for 18h; Inert atmosphere; Sealed tube;96%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

benzylamine
100-46-9

benzylamine

O-phenyl N-benzylcarbamate
22003-17-4

O-phenyl N-benzylcarbamate

Conditions
ConditionsYield
In tetrahydrofuran; water at 20℃; for 3h;99%
In tetrahydrofuran; water at 20℃; for 8h;85%
In neat (no solvent) at 80℃; for 0.166667h;
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

cis-1,2-cyclopentanediol
5057-98-7

cis-1,2-cyclopentanediol

(3aR,6aS)-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-2-one
87057-82-7

(3aR,6aS)-tetrahydro-3aH-cyclopenta[d][1,3]dioxol-2-one

Conditions
ConditionsYield
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In 2-methyltetrahydrofuran at 30℃; for 3h;99%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

4,4'-diamino diphenyl methane
101-77-9

4,4'-diamino diphenyl methane

N,N'-(4,4'-methanediyl-di-phenyl)-bis-carbamic acid diphenyl ester
101-65-5

N,N'-(4,4'-methanediyl-di-phenyl)-bis-carbamic acid diphenyl ester

Conditions
ConditionsYield
With zinc(II) acetate dihydrate at 50℃; Product distribution / selectivity; Industry scale;98.8%
With phenol; zinc(II) acetate dihydrate at 50℃; Product distribution / selectivity; Industry scale;98.8%
With isobutyric Acid; 1,3,5-tris(N,N-dimethylaminopropyl)-hexahydro-s-triazine In toluene at 55℃; for 48h;96.4%
With diphenyl-phosphinic acid at 89.85℃; for 7h; Acylation;91%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

4-methylbenzene-1,3-diamine
95-80-7

4-methylbenzene-1,3-diamine

toluene-2,4-dicarbamic acid diphenyl ester
4223-24-9

toluene-2,4-dicarbamic acid diphenyl ester

Conditions
ConditionsYield
With zinc(II) acetate dihydrate at 50℃; Industry scale;98.1%
With zinc(II) acetate dihydrate; phenol at 50℃; Industry scale;98.1%
With zinc(II) acetate dihydrate In phenol at 50℃;98.1%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

aniline
62-53-3

aniline

phenyl N-phenylcarbamate
4930-03-4

phenyl N-phenylcarbamate

Conditions
ConditionsYield
With isobutyric Acid; 1,3,5-tris(N,N-dimethylaminopropyl)-hexahydro-s-triazine In toluene at 55℃; for 48h;98%
With diphenyl-phosphinic acid In tetrahydrofuran at 69.9℃; for 20h;51%
With diphenyl-phosphinic acid In tetrahydrofuran at 89.84℃; for 20h;50%
With isobutyric Acid In neat (no solvent) at 80℃; for 4h; Inert atmosphere;
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

benzoic acid
65-85-0

benzoic acid

benzoic acid phenyl ester
93-99-2

benzoic acid phenyl ester

Conditions
ConditionsYield
With pyridine; dmap at 20℃; for 96h;98%
With pyridine at 140 - 150℃; for 6h; Esterification;92%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In neat (no solvent) at 160℃; for 24h; Green chemistry;73%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Cinnamic acid
621-82-9

Cinnamic acid

phenyl cinnamate
2757-04-2

phenyl cinnamate

Conditions
ConditionsYield
With pyridine; dmap at 20℃;98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

1h-benzotriazole-5-carboxylic acid
23814-12-2

1h-benzotriazole-5-carboxylic acid

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

5-phenoxycarbonylbenzotriazole
84902-17-0

5-phenoxycarbonylbenzotriazole

Conditions
ConditionsYield
With sodium carbonate98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

(αR)-2-amino-5-chloro-α-(2-cyclopropylethynyl)-α-(trifluoromethyl)benzenemethanol

(αR)-2-amino-5-chloro-α-(2-cyclopropylethynyl)-α-(trifluoromethyl)benzenemethanol

efavirenz
154598-52-4

efavirenz

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 60℃; for 2h;98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

(2S)-2-(2-amino-5-chlorophenyl)-4-cyclopropyl-1,1,1-trifluorobut-3-yn-2-ol
209414-27-7

(2S)-2-(2-amino-5-chlorophenyl)-4-cyclopropyl-1,1,1-trifluorobut-3-yn-2-ol

efavirenz
154598-52-4

efavirenz

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 20 - 60℃; for 2h;98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

4-[5-(4-(methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]benzenesulphonamide
169590-42-5

4-[5-(4-(methyl)phenyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]benzenesulphonamide

(Z)-4-(dimethylamino)-N-((4-(5-(p-tolyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)sulfonyl)pyridin-1-ium-1-carbimidate
1538566-50-5

(Z)-4-(dimethylamino)-N-((4-(5-(p-tolyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)sulfonyl)pyridin-1-ium-1-carbimidate

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.166667h;98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

N- [(4-fluorophenyl)methyl]-1-methylpiperidin-4-amine
359878-47-0

N- [(4-fluorophenyl)methyl]-1-methylpiperidin-4-amine

phenyl (4-fluorobenzyl)(1-methylpiperidin-4-yl)carbamate

phenyl (4-fluorobenzyl)(1-methylpiperidin-4-yl)carbamate

Conditions
ConditionsYield
In toluene at 20℃;98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

2-[2-(2-methoxyethoxy)ethoxy]ethylamine
74654-07-2

2-[2-(2-methoxyethoxy)ethoxy]ethylamine

N,N′-bis(3,6,9-trioxadecyl)urea

N,N′-bis(3,6,9-trioxadecyl)urea

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine for 3h; Reflux;98%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

1,4-phenylenediamine
106-50-3

1,4-phenylenediamine

1,4-phenylene bis-phenylcarbamate
22824-04-0

1,4-phenylene bis-phenylcarbamate

Conditions
ConditionsYield
With isobutyric Acid; 1,3,5-tris(N,N-dimethylaminopropyl)-hexahydro-s-triazine In toluene at 55℃; for 48h;98%
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