5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)

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Chemical Name:5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)
CAS No.:151422-07-0
Molecular Formula:C₅₂H₃₄Cl₇MnN₄O₃
Molecular Weight:1065.98
Hs Code.:

Synonyms:

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Chemical Property of 5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)

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Technology Process of 5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)

There total 1 articles about 5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5-(2-chloro-6-{7-(ethoxycarbonyl)heptyloxy}phenyl)-10,15,20-tris(2,6-dichlorophenyl)porphyrin

: 6156-78-1
manganese (II) acetate tetrahydrate

: 151422-07-0
5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)

Guidance literature:: In N,N-dimethyl-formamide; a soln. of porphyrin-compd. in DMF is stirred at reflux with Mn(OAc)2*4H2O for 6 h; evapn. under reduced pressure, the residue is dissolved in in CH2Cl2 and washed with water, evapn., the residue is dissolved in EtOH and NaOH and refluxed for 2 h, evapn., addn. of H2O and HCl, extn. with CH2Cl2, column chromy., dried over MgSO4;