6-amino-5-[(6-amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl)(phenyl)methyl]-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione

Base Information

• Chemical Name: 6-amino-5-[(6-amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl)(phenyl)methyl]-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione
• CAS No.: 13191-76-9
• Molecular Formula: C19H22N6O4
• Molecular Weight: 398.421
• Mol file: 13191-76-9.mol

Synonyms:

Chemical Property of 6-amino-5-[(6-amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl)(phenyl)methyl]-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione

Chemical Property:

• PSA: 140.04000
• LogP: -0.01160

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-amino-5-[(6-amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl)(phenyl)methyl]-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione

There total 6 articles about 6-amino-5-[(6-amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl)(phenyl)methyl]-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

6-Amino-1,3-dimethylbarbituric acid (6642-31-5) + benzaldehyde (100-52-7) → 6-amino-5-[6'-amino-1',3'-dimethyl-2',4'-dioxo-1',2',3',4'-tetrahydro-5'-pyrimidinyl(phenyl)methyl]-1,3-dimethyl-1,2,3,4-tetrahydro-2,4-pyrimidinedione (13191-76-9)

Guidance literature:

With hybrid material nanorod-[SiO₂-Pr-Im-SO₃H][TFA]; In ethanol; for 1h; Catalytic behavior; Reflux;

DOI:10.1007/s11164-020-04104-z

Reference yield: 84.0%

6-Amino-1,3-dimethylbarbituric acid (6642-31-5) + benzaldehyde (100-52-7) + acetylenedicarboxylic acid diethyl ester (762-21-0) → 6-amino-5-[6'-amino-1',3'-dimethyl-2',4'-dioxo-1',2',3',4'-tetrahydro-5'-pyrimidinyl(phenyl)methyl]-1,3-dimethyl-1,2,3,4-tetrahydro-2,4-pyrimidinedione (13191-76-9) + 1,3-dimethyl-2,4-dioxo-5-phenyl-1,2,3,4,5,8-hexahydropyrido[2,3-d]pyrimidine-6,7-dicarboxylic acid diethyl ester (1322078-67-0)

Guidance literature:

With L-proline; In ethanol; for 4h; Reflux;

DOI:10.1016/j.tet.2011.06.051

Reference yield: 54.0%

6-Amino-1,3-dimethylbarbituric acid (6642-31-5) + benzaldehyde (100-52-7) → 6-amino-5-[6'-amino-1',3'-dimethyl-2',4'-dioxo-1',2',3',4'-tetrahydro-5'-pyrimidinyl(phenyl)methyl]-1,3-dimethyl-1,2,3,4-tetrahydro-2,4-pyrimidinedione (13191-76-9) + 1,3,7,9-tetramethyl-5-phenylpyrido[2,3-d:6,5-d']dipyrimidine-2,4,6,8(1H,3H,7H,9H)-tetraone

Guidance literature:

toluene-4-sulfonic acid; In various solvent(s); at 100 ℃; for 4h;

DOI:10.1016/j.tet.2006.12.043

upstream raw materials:

6-Amino-1,3-dimethylbarbituric acid

benzaldehyde

S-benzylisothiourea hydrochloride

acetylenedicarboxylic acid diethyl ester

Downstream raw materials:

7-benzylthio-1,3-dimethyl-5-phenylpyrimido[4,5-d]pyrimidine-2,4-(1H,3H,5H,8H)-dione

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 13191-76-9 6-amino-5-[(6-amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-5-pyrimidinyl)(phenyl)methyl]-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione

Send

Send

Metric Ton KG G Pound L ML

Send

Send