3,5-Dimethy-D-Phenylalanine

Base Information

• Chemical Name: 3,5-Dimethy-D-Phenylalanine
• CAS No.: 1241680-65-8
• Molecular Formula: C₁₁H₁₅NO₂
• Molecular Weight: 193.246
• Mol file: 1241680-65-8.mol

Synonyms:

Chemical Property of 3,5-Dimethy-D-Phenylalanine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-Dimethy-D-Phenylalanine

There total 5 articles about 3,5-Dimethy-D-Phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetylamino-(3,5-dimethyl-benzyl)-malonic acid diethyl ester (109936-73-4) → DL-3,5-dimethylphenylalanine (103854-27-9,1241680-65-8)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/ja01572a065

Reference yield:

α-benzoylamino-4-iodo-3,5-dimethyl-trans-cinnamic acid ethyl ester → DL-3,5-dimethylphenylalanine (103854-27-9,1241680-65-8)

Guidance literature:

With phosphorus; hydrogen iodide; at 150 ℃;

DOI:10.1002/hlca.19520350736

Reference yield:

iodomesitylene (4028-63-1) → DL-3,5-dimethylphenylalanine (103854-27-9,1241680-65-8)

Guidance literature:

Multi-step reaction with 4 steps

1: MnO₂; aqueous H₂SO₄; CuSO₄

2: sodium acetate; acetic acid anhydride

3: ethanolic H₂SO₄

4: red phosphorus; aqueous HI / 150 °C

With manganese(IV) oxide; phosphorus; sulfuric acid; hydrogen iodide; sodium acetate; acetic anhydride; copper(II) sulfate;

DOI:10.1002/hlca.19520350736

upstream raw materials:

acetylamino-(3,5-dimethyl-benzyl)-malonic acid diethyl ester

iodomesitylene

4-iodo-3,5-dimethylbenzaldehyde