phenyl 2,3,4,5-tetrafluorobenzyl sulfone

Base Information

Chemical Name:phenyl 2,3,4,5-tetrafluorobenzyl sulfone
CAS No.:148203-92-3
Molecular Formula:C₁₃H₈F₄O₂S
Molecular Weight:304.265
Hs Code.:

Synonyms:

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Chemical Property of phenyl 2,3,4,5-tetrafluorobenzyl sulfone

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Technology Process of phenyl 2,3,4,5-tetrafluorobenzyl sulfone

There total 2 articles about phenyl 2,3,4,5-tetrafluorobenzyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53072-18-7
2,3,4,5-tetrafluorobenzyl alcohol

: 148203-92-3
phenyl 2,3,4,5-tetrafluorobenzyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

2: 2) monoperoxyphthalic acid Mg salt hexahydrate / 1) EtOH, 4 h, 2) 1 h

With magnesium monoperoxyphthalate hexahydrate; triethylamine; In dichloromethane;
DOI:10.1021/jo00062a030

Reference yield:

: 930-69-8
sodium thiophenolate

: Methanesulfonic acid 2,3,4,5-tetrafluoro-benzyl ester

: 148203-92-3
phenyl 2,3,4,5-tetrafluorobenzyl sulfone

Guidance literature:: With magnesium monoperoxyphthalate hexahydrate; Yield given. Multistep reaction; 1) EtOH, 4 h, 2) 1 h;
DOI:10.1021/jo00062a030

Reference yield:

: 148203-92-3
phenyl 2,3,4,5-tetrafluorobenzyl sulfone

: (+)-1,2-bis(2,3,4,5-tetrafluorophenyl)propane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-BuLi / 1) ether, hexane, 0 deg C, 2) ether, 0 deg C, 3 h

2: 96 percent / Raney Ni / ethanol / 4 h / Heating

With n-butyllithium; nickel; In ethanol;
DOI:10.1021/jo00062a030