1-Phenylazocane

Base Information

Chemical Name:1-Phenylazocane
CAS No.:131998-76-0
Molecular Formula:C13H19N
Molecular Weight:189.301
Hs Code.:
DSSTox Substance ID:DTXSID30570165
Nikkaji Number:J3.030.954E
Wikidata:Q82457527

Synonyms:1-Phenylazocane;1-Azacyclooctylbenzene;131998-76-0;SCHEMBL8542780;DTXSID30570165;GKCPYHQXCYWJBJ-UHFFFAOYSA-N

Suppliers and Price of 1-Phenylazocane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Phenylazocane

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:189.151749610
Heavy Atom Count:14
Complexity:141

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCCN(CCC1)C2=CC=CC=C2

Technology Process of 1-Phenylazocane

There total 7 articles about 1-Phenylazocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1121-92-2
heptamethyleneimine

: 108-86-1,52753-63-6
bromobenzene

: 131998-76-0
1-phenyloctahydroazocine

Guidance literature:: With sodium amide; In toluene; for 18h; Heating;

Reference yield: 79.0%

: 19858-03-8
1-phenyl-azocan-2-one

: 131998-76-0
1-phenyloctahydroazocine

Guidance literature:: With Dimethylphenylsilane; In ethyl acetate; at 20 - 80 ℃; for 26h; Green chemistry;
DOI:10.1002/adsc.201900838

Reference yield: 67.0%

: 1121-92-2
heptamethyleneimine

: 108-90-7
chlorobenzene

: 131998-76-0
1-phenyloctahydroazocine

Guidance literature:: With 5-(di-tert-butylphosphino)-1′, 3′, 5′-triphenyl-1′H-[1,4′]bipyrazole; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; sodium t-butanolate; In toluene; at 110 ℃; for 18h; Inert atmosphere; Glovebox;
DOI:10.1002/chem.201302453