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Technology Process of [Cr2(N,N'-bis(o-anisyl)formamidinate)4]

[Cr2(N,N'-bis(o-anisyl)formamidinate)4]

Base Information
  • Chemical Name:[Cr2(N,N'-bis(o-anisyl)formamidinate)4]
  • CAS No.:292642-61-6
  • Molecular Formula:C60H60Cr2N8O8
  • Molecular Weight:1125.18
  • Hs Code.:
[Cr<sub>2</sub>(N,N'-bis(o-anisyl)formamidinate)4]

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Chemical Property of [Cr2(N,N'-bis(o-anisyl)formamidinate)4]
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Technology Process of [Cr2(N,N'-bis(o-anisyl)formamidinate)4]

There total 1 articles about [Cr2(N,N'-bis(o-anisyl)formamidinate)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

chromium dichloride

chromium dichloride

N,N'-bis(2-methoxyphenyl)formamidine
68012-05-5

N,N'-bis(2-methoxyphenyl)formamidine

[Cr<sub>2</sub>(N,N'-bis(o-anisyl)formamidinate)4]
292642-61-6

[Cr2(N,N'-bis(o-anisyl)formamidinate)4]

Guidance literature:
With CH3Li; In tetrahydrofuran; diethyl ether; byproducts: LiCl; MeLi in Et2O was added dropwise to a suspn. of anhyd. CrCl2 in Et2O and ligand in THF, 3 h (N2 atm.); THF was removed in vac., washed with warm hexane, extd. with benzene, filtered, removed under vac.; crystd. from benzene-hexane; elem. anal.;
DOI:10.1039/b000329h
upstream raw materials:

N,N'-bis(2-methoxyphenyl)formamidine

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