C₁₉H₁₃N₅S

Base Information

Chemical Name:C₁₉H₁₃N₅S
CAS No.:1269467-50-6
Molecular Formula:C₁₉H₁₃N₅S
Molecular Weight:343.412
Hs Code.:

C<sub>19</sub>H<sub>13</sub>N<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₁₃N₅S

Chemical Property:

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Technology Process of C₁₉H₁₃N₅S

There total 9 articles about C₁₉H₁₃N₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₁₇ClN₄OS

: 1269467-50-6
C₁₉H₁₃N₅S

Guidance literature:: With hydrazine hydrate; In acetic acid; at 80 ℃;
DOI:10.1016/j.bmcl.2012.02.099

Reference yield:

: 104670-74-8
methyl 2-amino-3-bromobenzoate

: 1269467-50-6
C₁₉H₁₃N₅S

Guidance literature:: Multi-step reaction with 8 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / toluene / 100 °C

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / 1,4-dioxane; water / 100 °C

3: triethylamine; trichlorophosphate / acetonitrile / 100 °C

4: 1-methyl-pyrrolidin-2-one

5: water; sodium hydroxide / ethanol / 60 - 80 °C

6: ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 70 - 80 °C

7: 80 °C / Neat (no solvent)

8: hydrazine hydrate / acetic acid / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; potassium acetate; ammonium chloride; benzotriazol-1-ol; caesium carbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; ethanol; water; acetic acid; toluene; acetonitrile; 1: Miyaura borylation / 2: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.02.099

Reference yield:

: 1269467-96-0
methyl 2-amino-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 1269467-50-6
C₁₉H₁₃N₅S

Guidance literature:: Multi-step reaction with 7 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / 1,4-dioxane; water / 100 °C

2: triethylamine; trichlorophosphate / acetonitrile / 100 °C

3: 1-methyl-pyrrolidin-2-one

4: water; sodium hydroxide / ethanol / 60 - 80 °C

5: ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 70 - 80 °C

6: 80 °C / Neat (no solvent)

7: hydrazine hydrate / acetic acid / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; ammonium chloride; benzotriazol-1-ol; caesium carbonate; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; trichlorophosphate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; ethanol; water; acetic acid; acetonitrile; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.02.099