1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene

Base Information

Chemical Name:1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene
CAS No.:913059-06-0
Molecular Formula:C₄₀H₃₆B₂O
Molecular Weight:554.347
Hs Code.:

Synonyms:

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Chemical Property of 1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene

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Technology Process of 1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene

There total 2 articles about 1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 95072-98-3
10-bromo-9-oxa-10-boradihydroanthracene

: tetrakis(tetrahydrofuran)lithium dimesityl-1,8-naphthalenediylborate

: 913059-06-0
1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene

Guidance literature:: In diethyl ether; soln. of OC12H8BBr in Et2O added to suspn. of Li salt of naphthalendiylborate in Et2O at 25°C; stirred at room temp. for 2 h; filtered; solvent removed from filtrate under vac.; extd. with CH2Cl2; filtered; solvent evapd.; washed with EtOH; dried under vac.; recrystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1021/ic060709s

Reference yield:

: 18055-73-7
bis[2-(trimethylsilanyl)phenyl] ether

: 913059-06-0
1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: diethyl ether

In diethyl ether; dichloromethane;
DOI:10.1021/ic060709s

Reference yield: 85.0%

: 913059-06-0
1-(dimesitylboryl)-8-(10'-bora-9'-oxaanthryl)naphthalene

: 150746-76-2
tris(dimethylamino)sulfonium trimethylsilyldifluoride

Guidance literature:: In tetrahydrofuran; soln. of (Me3SiF2)(S(NMe2)3) in THF added to soln. of B compd. in THF at25°C; 15 min; solvent evapd.; washed with Et2O; dried under vac.; crystd. by slow evapn. of MeCN soln.; elem. anal.;
DOI:10.1021/ic060709s