(Oxybis(2,1-phenylene))bis(trimethylsilane)

Base Information

Chemical Name:(Oxybis(2,1-phenylene))bis(trimethylsilane)
CAS No.:18055-73-7
Molecular Formula:C₁₈H₂₆OSi₂
Molecular Weight:314.575
Hs Code.:
European Community (EC) Number:659-925-9

Synonyms:(Oxybis(2,1-phenylene))bis(trimethylsilane);18055-73-7;SCHEMBL10998389;AKOS024338616;trimethyl{2-[2-(trimethylsilyl)phenoxy]phenyl}silane

Suppliers and Price of (Oxybis(2,1-phenylene))bis(trimethylsilane)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
(OXYDI-2,1-PHENYLENE)BIS(TRIMETHYLSILANE) Aldrich
1ea
$ 57.00

Total 4 raw suppliers

Chemical Property of (Oxybis(2,1-phenylene))bis(trimethylsilane)

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:314.15221852
Heavy Atom Count:21
Complexity:297

Purity/Quality:

98%,99%, ^*data from raw suppliers

(OXYDI-2,1-PHENYLENE)BIS(TRIMETHYLSILANE) Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C)C1=CC=CC=C1OC2=CC=CC=C2[Si](C)(C)C

Technology Process of (Oxybis(2,1-phenylene))bis(trimethylsilane)

There total 2 articles about (Oxybis(2,1-phenylene))bis(trimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101-84-8
diphenylether

: 18055-73-7
bis[2-(trimethylsilanyl)phenyl] ether

Guidance literature:: With n-butyllithium; nachfolgende Umsetzung mit Chlor-trimethyl-silan;
DOI:10.1021/jo01103a036

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 101-84-8
diphenylether

: 18055-73-7
bis[2-(trimethylsilanyl)phenyl] ether

Guidance literature:: Multistep reaction; (i) nBuLi, (ii) /BRN= 1209232/;
DOI:10.1002/hlca.19730560127

Reference yield:

: 18055-73-7
bis[2-(trimethylsilanyl)phenyl] ether

: C₃₁H₂₇BN₂O

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / -78 - 20 °C / Inert atmosphere

2.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.joc.7b02602