Technology Process of C47H56BNOS2
There total 5 articles about C47H56BNOS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere
1.2: -78 - 25 °C / Inert atmosphere
2.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate / toluene / Inert atmosphere; Reflux
3.1: hydrogenchloride / methanol / Reflux
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; potassium phosphate; n-butyllithium; palladium diacetate;
In
tetrahydrofuran; methanol; hexane; toluene;
DOI:10.1039/c0cc04573j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate / toluene / Inert atmosphere; Reflux
2: hydrogenchloride / methanol / Reflux
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; potassium phosphate; palladium diacetate;
In
methanol; toluene;
DOI:10.1039/c0cc04573j