Technology Process of isobutyl 3,7,11,15-tetramethylhexadeca-2,4,6,8-tetraenoate
There total 6 articles about isobutyl 3,7,11,15-tetramethylhexadeca-2,4,6,8-tetraenoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ISOPROPYLAMIDE;
In
chloroform;
at 30 ℃;
for 2h;
Yield given;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium isobutoxide / diethyl ether; toluene / 0.5 h / -20 °C
2: 17percent aq. HCl / diethyl ether; toluene; acetone / 1 h / Ambient temperature
3: PBr3 / diethyl ether / 1 h / 20 °C
4: dimethylacetamide / CHCl3 / 2 h / 30 °C
With
hydrogenchloride; ISOPROPYLAMIDE; potassium 2-methylpropan-2-olate; phosphorus tribromide;
In
diethyl ether; chloroform; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium isobutoxide / diethyl ether; toluene / 0.5 h / -20 °C
2: 17percent aq. HCl / diethyl ether; toluene; acetone / 1 h / Ambient temperature
3: PBr3 / diethyl ether / 1 h / 20 °C
4: dimethylacetamide / CHCl3 / 2 h / 30 °C
With
hydrogenchloride; ISOPROPYLAMIDE; potassium 2-methylpropan-2-olate; phosphorus tribromide;
In
diethyl ether; chloroform; acetone; toluene;