(Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O

Base Information

Chemical Name:(Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O
CAS No.:146467-97-2
Molecular Formula:C₃₂H₃₂CuN₄O₆P₂*H₂O
Molecular Weight:712.138
Hs Code.:

(Cu(C<sub>6</sub>H<sub>5</sub>PO<sub>3</sub>H)2(C<sub>5</sub>H<sub>5</sub>N)4)*H<sub>2</sub>O

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Chemical Property of (Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O

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Technology Process of (Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O

There total 2 articles about (Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: tetrakis(acetato)diaquadicopper(II)

: 1571-33-1
phenylphosphonate

: 146467-97-2
(Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O

Guidance literature:: In pyridine; addn. of PhPO(OH)2 to a dark-blue soln. of Cu-complex in pyridine, refluxing mixt. for 4 h, colour changes to mint green, further reflux for 24 h; cooling to room temp., pptn., filtn., washing with Et2O, drying in vacuo, elem. anal.;
DOI:10.1016/S0277-5387(00)83649-9

Reference yield: 22.0%

: tetrakis(acetato)diaquadicopper(II)

: 1779-48-2
phenylphosphinic acid

: 146467-97-2
(Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O

Guidance literature:: With air; In pyridine; addn. of PhPHOOH to Cu-complex in pyridine (room temp., under N2), stirring for 3 h to give a light yellow soln., exposing to air, colour changes to mint green within 20 min, deoxygenating (N2), soln. turns yellow, stirring green soln. (air, 2 d), pptn.; filtn., washing with Et2O, drying in vacuo, elem. anal.;
DOI:10.1016/S0277-5387(00)83649-9

Reference yield:

: 146467-97-2
(Cu(C₆H₅PO₃H)2(C₅H₅N)4)*H₂O

: (Cu(C₆H₅PO₃H)2(C₅H₅N)4)*2CH₃OH

Guidance literature:: With CH₃OH; In pyridine; methanol; recrystn. of Cu-complex from a 50:50 mixt. of pyridine and methanol;
DOI:10.1016/S0277-5387(00)83649-9