5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester

Base Information

Chemical Name:5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester
CAS No.:856651-70-2
Molecular Formula:C₁₉H₂₆O₆
Molecular Weight:350.412
Hs Code.:

Synonyms:

Suppliers and Price of 5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester

There total 2 articles about 5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773094-77-2
2-(3,5-dibromophenyl)-1,3-dioxolane

: 201230-82-2
carbon monoxide

: 71-36-3
butan-1-ol

: 856651-70-2
5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; at 90 ℃; for 48h; under 1520 Torr;
DOI:10.1021/jo047741t

Reference yield:

: 56990-02-4
3,5-dibromobenzaldehyde

: 856651-70-2
5-[1,3]dioxolan-2-yl-isophthalic acid dibutyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / benzene / 5 h / Heating

2: PPh₃; Pd(PPh₃)4; triethylamine / 48 h / 90 °C / 1520 Torr

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; In benzene;
DOI:10.1021/jo047741t