diphenyldi(p-tolyl)germane

Base Information

Chemical Name:diphenyldi(p-tolyl)germane
CAS No.:171361-04-9
Molecular Formula:C₂₆H₂₄Ge
Molecular Weight:409.067
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyldi(p-tolyl)germane

Chemical Property:

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Technology Process of diphenyldi(p-tolyl)germane

There total 4 articles about diphenyldi(p-tolyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.1%

: 352-32-9
p-fluorotoluene

: 100184-59-6
diphenylgermylenedipotassium

: diphenyl(p-tolyl)germane

: 171361-04-9
diphenyldi(p-tolyl)germane

: 1675-58-7
diphenylgermane

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to p-MeC6H4F in THF, stirred at roomtemp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443

Reference yield: 45.9%

: 100184-59-6
diphenylgermylenedipotassium

: 106-43-4
para-chlorotoluene

: diphenyl(p-tolyl)germane

: 171361-04-9
diphenyldi(p-tolyl)germane

: 1675-58-7
diphenylgermane

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to p-MeC6H4Cl in THF, stirred at room temp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443

Reference yield: 17.0%

: (p-tolyl)magnesium bromide

: 1613-66-7
dichlorodiphenylgermane

: 171361-04-9
diphenyldi(p-tolyl)germane

Guidance literature:: In diethyl ether; toluene; stirring (room temp., 2 h), refluxing (16 h); recrystn. (MeOH); elem. anal.;
DOI:10.1016/0277-5387(95)00069-5