3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Base Information

Chemical Name:3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester
CAS No.:116527-89-0
Molecular Formula:C₄₃H₄₉N₃O₆
Molecular Weight:703.879
Hs Code.:

3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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Chemical Property of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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Technology Process of 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

There total 10 articles about 3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116527-79-8,116527-80-1
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol

: 116527-89-0
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

2: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

3: triethylamine, tert.-butylhypochlorite / CCl₄; CH₂Cl₂ / 0 °C

4: silver tetrafluoroborate / CH₂Cl₂; acetonitrile / 1 h / Heating

With hydrogenchloride; silver tetrafluoroborate; tert-butylhypochlorite; water; triethylamine; In tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116527-89-0
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

3: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

4: triethylamine, tert.-butylhypochlorite / CCl₄; CH₂Cl₂ / 0 °C

5: silver tetrafluoroborate / CH₂Cl₂; acetonitrile / 1 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; silver tetrafluoroborate; tert-butylhypochlorite; water; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-74-3,116527-77-6
2-(3-benzyloxypropyl)-3-oxo-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-2-carbonsaure

: 116527-89-0
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-7-(4-dimethylamino-2-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / 200 - 210 °C

2: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

3: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

4: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

5: triethylamine, tert.-butylhypochlorite / CCl₄; CH₂Cl₂ / 0 °C

6: silver tetrafluoroborate / CH₂Cl₂; acetonitrile / 1 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; silver tetrafluoroborate; tert-butylhypochlorite; water; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)86862-9