Benzene, 1-[(1E)-2-(4-methoxyphenyl)ethenyl]-4-(trifluoromethyl)-

Base Information

Chemical Name:Benzene, 1-[(1E)-2-(4-methoxyphenyl)ethenyl]-4-(trifluoromethyl)-
CAS No.:132312-99-3
Molecular Formula:C16H13F3O
Molecular Weight:278.274
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-[(1E)-2-(4-methoxyphenyl)ethenyl]-4-(trifluoromethyl)-

Chemical Property:

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Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Benzene, 1-[(1E)-2-(4-methoxyphenyl)ethenyl]-4-(trifluoromethyl)-

There total 24 articles about Benzene, 1-[(1E)-2-(4-methoxyphenyl)ethenyl]-4-(trifluoromethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 40474-01-9
1-methoxy-4-((4-(trifluoromethyl)phenyl)ethynyl)benzene

: 132312-99-3
1-methoxy-4-[(E)-2-[4-(trifluoromethyl)phenyl]ethenyl]benzene

Guidance literature:: With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); formic acid; In toluene; Flow reactor;
DOI:10.1021/acscatal.6b01045

Reference yield: 90.0%

: 455-13-0
4-Iodobenzotrifluoride

: 6303-59-9,60592-52-1,27570-08-7
(E)-4-(2-bromo-vinyl)-anisole

: 132312-99-3
1-methoxy-4-[(E)-2-[4-(trifluoromethyl)phenyl]ethenyl]benzene

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 4,4'-di-tert-butyl-2,2'-bipyridine; lithium chloride; magnesium chloride; zinc; In tetrahydrofuran; at 0 - 20 ℃; for 15h; chemoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201607959

Reference yield: 88.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 128796-39-4
4-trifluoromethylphenylboronic acid

: 132312-99-3
1-methoxy-4-[(E)-2-[4-(trifluoromethyl)phenyl]ethenyl]benzene

Guidance literature:: With potassium fluoride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonato)palladium(II); propionic acid; at 20 ℃; for 2h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201108211