(2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

Base Information

Chemical Name:(2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione
CAS No.:143893-02-1
Molecular Formula:C₂₈H₃₀O₆S
Molecular Weight:494.609
Hs Code.:

(2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of (2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

There total 1 articles about (2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 125108-66-9
furaquinocin A

: 882-33-7
diphenyldisulfane

: 143893-02-1
(2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

Guidance literature:: With tributylphosphine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)91714-3

Reference yield: 19.0%

: 143893-02-1
(2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

: 134984-99-9
furaquinocin D

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;
DOI:10.1016/S0040-4039(00)91714-3

Reference yield:

: 143893-02-1
(2R,3S)-4-Hydroxy-3-((Z)-(R)-1-hydroxy-4-methyl-5-phenylsulfanyl-pent-3-enyl)-7-methoxy-2,3,8-trimethyl-2,3-dihydro-naphtho[1,2-b]furan-6,9-dione

: (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (R)-1-[(2R,3R)-7-methoxy-2,3,8-trimethyl-6,9-dioxo-4-((R)-3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-2,3,6,9-tetrahydro-naphtho[1,2-b]furan-3-yl]-4-methyl-pent-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / n-Bu₃SnH, AIBN / benzene / Heating

2: DCC, DMAP / CH₂Cl₂ / Ambient temperature

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; dicyclohexyl-carbodiimide; In dichloromethane; benzene;
DOI:10.1016/S0040-4039(00)91714-3