(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride

Base Information

Chemical Name:(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride
CAS No.:255727-75-4
Molecular Formula:C₂₀H₁₈BiCl₃O
Molecular Weight:589.702
Hs Code.:

Synonyms:

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Chemical Property of (4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride

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Technology Process of (4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride

There total 1 articles about (4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7791-25-5
sulfuryl dichloride

: 175546-50-6
(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuthane

: 255727-75-4
(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride

Guidance literature:: In dichloromethane; Ar-atmosphere; SO2Cl2 addn. (0°C), stirring (2-3 h); evapn. (vac.); elem. anal.;
DOI:10.1021/om990597v

Reference yield: 66.0%

: 7789-23-3
potassium fluoride

: 255727-75-4
(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride

: 255727-78-7
(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth difluoride

Guidance literature:: In ethanol; water; Ar-atmosphere; KF excess; stirring (12 h, room temp.), diln. with H2O, EtOH evapn. (vac.), extn. (CH2Cl2), org. phase evapn. (vac.), H2O/EtOH addn., KF addn. (excess), stirring (6 h); diln. with H2O, EtOH evapn. (vac.), extn. (CH2Cl2), org. phase evapn. (vac.), recrystn. (CH2Cl2/hexane 1/5); elem. anal.;
DOI:10.1021/om990597v

Reference yield:

: 255727-75-4
(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)bismuth dichloride

: 203342-16-9
(4-chlorophenyl)(2-methoxyphenyl)(4-methylphenyl)(4-methylthiophenyl)bismuthonium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: water; ethanol

2: Me₃SiCN / dichloromethane

With Me₃SiCN; In ethanol; dichloromethane; water;
DOI:10.1021/om990597v