[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

Base Information

Chemical Name:[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene
CAS No.:705269-75-6
Molecular Formula:C₂₄H₃₆O₆P₂PbS
Molecular Weight:721.76
Hs Code.:

Synonyms:

Suppliers and Price of [4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

There total 4 articles about [4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 705269-73-4
[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]chloroplumbylene

: 930-69-8
sodium thiophenolate

: 705269-75-6
[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; NaSC6H5 added portionswise at -78 °C under argon to a suspension of the starting Pb-complex, stirred for 16 h (-78 °C to room temp.); decanted from the insoluble residue, solution kept at -6 °C, elem. anal.;
DOI:10.1002/ejic.200300139

Reference yield:

: 705269-84-7
[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]chloroplumbylene*tetrahydrofuran

: 705269-75-6
[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent)

2: tetrahydrofuran

In tetrahydrofuran;
DOI:10.1002/ejic.200300139

Reference yield:

: [(2,6-Bis(diethoxyphosphonyl)-4-tert-butyl)phenyl]lithium

: 705269-75-6
[4-tert-butyl-2,6-bis(diethoxyphosphonyl)phenyl]thiophenolatoplumbylene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: neat (no solvent)

3: tetrahydrofuran

In tetrahydrofuran;
DOI:10.1002/ejic.200300139