(Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

Base Information

Chemical Name:(Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester
CAS No.:146038-31-5
Molecular Formula:C₄₀H₆₇F₅O₇Si₃
Molecular Weight:839.216
Hs Code.:

(Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

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Chemical Property of (Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

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Technology Process of (Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

There total 4 articles about (Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67910-12-7
11-Dehydrothromboxane B₂

: 146038-31-5
(Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 1) NH₄HCO₃, pyridine, 2) i-Pr₂NEt / 1) 3 h, r.t., 2) MeCN, 40 deg C, 30 min

3: pyridine / 0.25 h / 40 °C

With pyridine; ammonium bicarbonate; N-ethyl-N,N-diisopropylamine; In diethyl ether;
DOI:10.1002/oms.1210271130

Reference yield:

: 62365-34-8
N-dimethylethylsilyl-imidazole

: (Z)-(8S,9S)-8-((E)-(1R,4S)-1,4-Dihydroxy-non-2-enyl)-9-hydroxy-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

: 146038-31-5
(Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

Guidance literature:: With pyridine; at 40 ℃; for 0.25h;
DOI:10.1002/oms.1210271130

Reference yield:

: 67719-11-3
11-Dehydrothromboxane B₂ methyl ester

: 146038-31-5
(Z)-(8S,9S)-8-[(E)-(1R,4S)-1,4-Bis-(ethyl-dimethyl-silanyloxy)-non-2-enyl]-9-(ethyl-dimethyl-silanyloxy)-undec-5-enedioic acid 1-methyl ester 11-pentafluorophenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NH₄HCO₃, pyridine, 2) i-Pr₂NEt / 1) 3 h, r.t., 2) MeCN, 40 deg C, 30 min

2: pyridine / 0.25 h / 40 °C

With pyridine; ammonium bicarbonate; N-ethyl-N,N-diisopropylamine;
DOI:10.1002/oms.1210271130