cylohexenylacetylenehexacarbonyldicobalt

Base Information

Chemical Name:cylohexenylacetylenehexacarbonyldicobalt
CAS No.:40747-50-0
Molecular Formula:C₁₄H₁₀Co₂O₆
Molecular Weight:392.216
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cylohexenylacetylenehexacarbonyldicobalt

Chemical Property:

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Technology Process of cylohexenylacetylenehexacarbonyldicobalt

There total 1 articles about cylohexenylacetylenehexacarbonyldicobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 931-49-7
1-ethenylcyclohexene

: 40747-50-0
cylohexenylacetylenehexacarbonyldicobalt

Guidance literature:: In benzene; Ar atmosphere; mixing of solns. of educts, stirring (2 h, 20°C); filtration (Al2O3 layer), removal of benzene (evepn.), extn. (hexane), filtration (layer Al2O3), removal of hexane;
DOI:10.1007/BF00948643

Reference yield: 95.0%

: 40747-50-0
cylohexenylacetylenehexacarbonyldicobalt

: 2-Methyl-3-chloropropionyl tetrafluoroborate

: 135414-00-5,135413-99-9,135414-02-7,135414-01-6,122953-66-6
C₆H₉(OCH₃)(C(O)CH(CH₃)CH₂Cl)CCHCo₂(CO)6

Guidance literature:: With methanol; G. S. Mikaelyan, V. A. Smit, A. S. Batsanov, and Yu. T. Struchkov, Izv. Akad. Nauk SSSR, Ser. Khim., No. 9, 2105 (1984);
DOI:10.1007/BF00953659

Reference yield: 71.0%

: 40747-50-0
cylohexenylacetylenehexacarbonyldicobalt

: 352-66-9
3-methylbutyroyl fluoride

: 107-18-6
allyl alcohol

: 108448-62-0,94927-46-5
Co₂(CO)6HCCC₆H₉(OCH₂CHCH₂)(COCH₂CH(CH₃)2)

Guidance literature:: With boron trifluoride; potassium carbonate; In dichloromethane; addn. of soln. of vinylacetylene complex to soln. of acyl fluoride, ca -70°C, stirring, addn. of BF3, addn. of allyl alcohol and K2CO3;
DOI:10.1007/BF00953615