(iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)

Base Information

Chemical Name:(iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)
CAS No.:32629-80-4
Molecular Formula:C₇₂H₆₀As₄Cl₂FeO₄*Cl₄Fe
Molecular Weight:1613.36
Hs Code.:

(iron(III)(triphenylarsine oxide)4Cl<sub>2</sub>)(FeCl<sub>4</sub>)

Synonyms:

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Chemical Property of (iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)

Chemical Property:

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Technology Process of (iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)

There total 2 articles about (iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1153-05-5,856568-31-5
triphenylarsineoxide

: 7705-08-0
iron(III) chloride

: [Fe₂O(triphenylarsine oxide)4Cl₃][FeCl₄] * MeCN

: 72377-35-6,32629-80-4
(iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)

: 2Fe₂O(OAs(C₆H₅)3)4Cl₃⁽¹⁺⁾*Fe₂OCl₆^(2-)*2CH₃CN=[Fe₂O(OAs(C₆H₅)3)4Cl₃]2[Fe₂OCl₆]*2CH₃CN

Guidance literature:: In ethanol; stirring (room temp., 2 h); filtering, recrystn. (MeCN); elem. anal.;
DOI:10.1016/S0277-5387(98)00094-1

Reference yield:

: 603-32-7
triphenyl-arsane

: 80937-33-3
oxygen

: 7705-08-0
iron(III) chloride

: [Fe₂O(triphenylarsine oxide)4Cl₃][FeCl₄] * MeCN

: 72377-35-6,32629-80-4
(iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)

: 2Fe₂O(OAs(C₆H₅)3)4Cl₃⁽¹⁺⁾*Fe₂OCl₆^(2-)*2CH₃CN=[Fe₂O(OAs(C₆H₅)3)4Cl₃]2[Fe₂OCl₆]*2CH₃CN

Guidance literature:: In acetonitrile; O2-atmosphere; stirring (333 K, 2 d); filtering, fractional crystn. (MeCN);
DOI:10.1016/S0277-5387(98)00094-1

Reference yield:

: 72377-35-6,32629-80-4
(iron(III)(triphenylarsine oxide)4Cl₂)(FeCl₄)

: (iron(III)(triphenylarsine oxide)4(OS(O)Cl)2)(FeCl₄)

Guidance literature:: With SO₂; In neat (no solvent, solid phase); complex in the solid state is placed in a dry Rotaflo tube, filled with argon, vac. is applied and removed with 1 atm SO2, more SO2 is added daily until constant mass is reached; mass of SO2 absorbed by the complex is determined;
DOI:10.1039/DT9900002657