bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)

Base Information

Chemical Name:bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)
CAS No.:138270-73-2
Molecular Formula:C₃₂H₃₄CoIO₄P₂
Molecular Weight:730.465
Hs Code.:

Synonyms:

Suppliers and Price of bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)

Chemical Property:

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Technology Process of bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)

There total 1 articles about bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73785-74-7
(diphenylphosphino)acetaldehyde ethylene acetal

: 138270-73-2
bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; isopropyl alcohol

2: tetrahydrofuran

In tetrahydrofuran; methanol; isopropyl alcohol;

Reference yield:

: 138270-73-2
bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P;O,P}iodocobalt(I)

: bis{(1,3-dioxolanyl-2-methyl)diphenylphosphane-P}(dicarbonyl)iodocobalt(I)

Guidance literature:: With CO; In tetrahydrofuran; exclusion of air and moisture, under purified Ar; a dry stream of CO is bubbled through a soln. of the Co-compd. in THF at -40°C for 15 min, warming up to room temp. and removing of the solvent in vac.; the residue is dissolved in ethanol, pptn. by cooling down to -30°C, the ppt. is filtered off and dried in vac.for 4 h, elem. anal.;