Technology Process of C29H49N3O8Si
There total 4 articles about C29H49N3O8Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1002/chem.201203667
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1002/chem.201203667
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1002/chem.201203667
