MoCl₄(dppm)

Base Information

Chemical Name:MoCl₄(dppm)
CAS No.:122068-49-9
Molecular Formula:C₂₅H₂₂Cl₄MoP₂
Molecular Weight:622.149
Hs Code.:

Synonyms:

Suppliers and Price of MoCl₄(dppm)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of MoCl₄(dppm)

Chemical Property:

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Technology Process of MoCl₄(dppm)

There total 1 articles about MoCl₄(dppm) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.8%

: 56613-96-8,77210-60-7,15584-93-7,19187-82-7
bis(acetonitrile)tetrachloromolybdenum(IV)

: 2071-20-7
bis-diphenylphosphinomethane

: 122068-49-9
MoCl₄(dppm)

Guidance literature:: In benzene; addn. of MoCl4(CH3CN)2 to a soln. of PPh2CH2PPh2 in dry benzene, heating under reflux under N2 (2 h), cooling, pptn.; filtration, washing (benzene);

Reference yield: 10.0%

: 122068-49-9
MoCl₄(dppm)

: 603-35-0
triphenylphosphine

: 122068-47-7
Mo(η6-PhPPh2)(dppm)(PPh3)

Guidance literature:: With Na/Hg amalgam; In tetrahydrofuran; dissolving of PPh3 in double-distd. THF under Ar, addn. of MoCl4(dppm), vigorous stirring (5 min), addn. of Na/Hg amalgam, thorough degassing, color change from brown, red, dirty green to brown (during the first 15 min), vigorous stirring (2 h); sepn. from Na/Hg by a cannula, filtration (Celite), reducing of vol., dropwise addn. of methanol to a dark reddish brown air-sensitive product, dissolving in benzene, chromy. (Al2O3 under N2), crystn. (benzene/methanol); elem. anal.;

Reference yield:

: 122068-49-9
MoCl₄(dppm)

: 1486-28-8
diphenyl(methyl)phosphine

: 122092-56-2
Mo(η6-PhPMePh)(dppm)(PMePh2)

Guidance literature:: With Na/Hg amalgam; In tetrahydrofuran; redn. of the corresponding tetrachloride with Na/Hg amalgam in the presence of excess PPh2Me in THF soln. under Ar;