(C₅H₄Si(C₆H₅)3)(CO)2ReH₂

Base Information

Chemical Name:(C₅H₄Si(C₆H₅)3)(CO)2ReH₂
CAS No.:105795-83-3
Molecular Formula:C₂₅H₂₁O₂ReSi
Molecular Weight:567.733
Hs Code.:

(C<sub>5</sub>H<sub>4</sub>Si(C<sub>6</sub>H<sub>5</sub>)3)(CO)2ReH<sub>2</sub>

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Chemical Property of (C₅H₄Si(C₆H₅)3)(CO)2ReH₂

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Technology Process of (C₅H₄Si(C₆H₅)3)(CO)2ReH₂

There total 4 articles about (C₅H₄Si(C₆H₅)3)(CO)2ReH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: (C₅H₅)(CO)2Re(Si(C₆H₅)3)H

: 105795-83-3,105880-03-3
(C₅H₄Si(C₆H₅)3)(CO)2ReH₂

Guidance literature:: With trifluoromethanesulphonic acid or F₃CCOOH; neopentyllithium; In tetrahydrofuran; under Ar, Re complex soln. cooled to -78°C, treated with neopentyllithium, stirred for 15 min, warmed to room temp., treated with F3CSO3H or F3CCOOH; removal of solvent in vac., residue taken up in hexane/CH2Cl2, filtration, removal of solvents, recrystn. (hexane), elem.anal.;
DOI:10.1016/0022-328X(86)80037-7

Reference yield:

: 105795-82-2
(C₅H₄Si(C₆H₅)3)(CO)2ReH^(1-)*Li⁽¹⁺⁾=[(C₅H₄Si(C₆H₅)3)(CO)2ReH]Li

: 105795-83-3,105880-03-3
(C₅H₄Si(C₆H₅)3)(CO)2ReH₂

: 105795-83-3,105880-03-3
(C₅H₄Si(C₆H₅)3)(CO)2ReH₂

Guidance literature:: With trifluoromethanesulphonic acid or F₃CCOOH; In tetrahydrofuran; under Ar at room temp.;
DOI:10.1016/0022-328X(86)80037-7

Reference yield:

: 105795-82-2
(C₅H₄Si(C₆H₅)3)(CO)2ReH^(1-)*Li⁽¹⁺⁾=[(C₅H₄Si(C₆H₅)3)(CO)2ReH]Li

: 105795-83-3,105880-03-3
(C₅H₄Si(C₆H₅)3)(CO)2ReH₂

: 105795-83-3,105880-03-3
(C₅H₄Si(C₆H₅)3)(CO)2ReH₂

Guidance literature:: With trifluoromethanesulphonic acid or F₃CCOOH; In tetrahydrofuran; under Ar at room temp.;
DOI:10.1016/0022-328X(86)80037-7