3,5-dinitro-2,4-dicyclopropylanisole

Base Information

Chemical Name:3,5-dinitro-2,4-dicyclopropylanisole
CAS No.:81484-58-4
Molecular Formula:C₁₃H₁₄N₂O₅
Molecular Weight:278.265
Hs Code.:

Synonyms:

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Chemical Property of 3,5-dinitro-2,4-dicyclopropylanisole

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Technology Process of 3,5-dinitro-2,4-dicyclopropylanisole

There total 3 articles about 3,5-dinitro-2,4-dicyclopropylanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.1%

: 81484-45-9
2,4-dicyclopropylanisole

: 81484-51-7
5-nitro-2,4-dicyclopropylanisole

: 81484-58-4
3,5-dinitro-2,4-dicyclopropylanisole

Guidance literature:: With nitric acid; acetic anhydride; at -50 ℃; for 2h;

Reference yield:

: 10292-66-7
1-cyclopropyl-2-methoxybenzene

: 81484-58-4
3,5-dinitro-2,4-dicyclopropylanisole

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / aluminum chloride / CHCl₃ / -65 °C

2: 1.)(C₂H₅)2NH_.HCl; CH₂O; 2.)N₂H_4.H₂O; KOH; 3.)KOH/Ag; Pt/C;

3: 46.1 percent Turnov_. / acetic anhydride, HNO₃ (d=1.52) / 2 h / -50 °C

With potassium hydroxide; platinum on activated charcoal; formaldehyd; aluminium trichloride; nitric acid; diethyl amine hydrochloride; silver; acetic anhydride; hydrazine hydrate; In chloroform;

Reference yield:

: 81484-47-1
1-(3-cyclopropyl-4-methoxyphenyl)ethan-1-one

: 81484-58-4
3,5-dinitro-2,4-dicyclopropylanisole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.)(C₂H₅)2NH_.HCl; CH₂O; 2.)N₂H_4.H₂O; KOH; 3.)KOH/Ag; Pt/C;

2: 46.1 percent Turnov_. / acetic anhydride, HNO₃ (d=1.52) / 2 h / -50 °C

With potassium hydroxide; platinum on activated charcoal; formaldehyd; nitric acid; diethyl amine hydrochloride; silver; acetic anhydride; hydrazine hydrate;