3-diphenylstibino-3',4'-dimethyltetrathiafulvalene

Base Information

Chemical Name:3-diphenylstibino-3',4'-dimethyltetrathiafulvalene
CAS No.:498552-08-2
Molecular Formula:C₂₀H₁₇S₄Sb
Molecular Weight:507.369
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-diphenylstibino-3',4'-dimethyltetrathiafulvalene

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Technology Process of 3-diphenylstibino-3',4'-dimethyltetrathiafulvalene

There total 1 articles about 3-diphenylstibino-3',4'-dimethyltetrathiafulvalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 62024-60-6
3,4-dimethyltetrathiafulvalene

: 2629-47-2
diphenylantimony(III) chloride

: 498552-08-2
3-diphenylstibino-3',4'-dimethyltetrathiafulvalene

Guidance literature:: With nBuLi; diisopropylamine; In diethyl ether; hexane; diisopropylamine and nBuLi in hexane were added to soln. of ligand in Et2O at -78°C, stirred for 2 h at -78°C, treated with SbClPh2 in Et2O, warmed to room temp., stirred overnight; filtered through silica gel with toluene, solvent was removed, sublimed at 75°C, recrystd. from Et2O; elem. anal.;
DOI:10.1039/b205594p