TZ-9

Base Information

Chemical Name:TZ-9
CAS No.:1002789-86-7
Molecular Formula:C₁₇H₁₄N₆O₄
Molecular Weight:366.336
Hs Code.:
Mol file:1002789-86-7.mol

Synonyms:

Suppliers and Price of TZ-9

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
SMI#9
1mg
$ 90.00

DC Chemicals
TZ9 >98%
100 mg
$ 700.00

DC Chemicals
TZ9 >98%
250 mg
$ 1400.00

Crysdot
TZ9 98+%
50mg
$ 483.00

Crysdot
TZ9 98+%
5mg
$ 77.00

Crysdot
TZ9 98+%
10mg
$ 126.00

ChemScene
TZ9 99.65%
5mg
$ 132.00

ChemScene
TZ9 99.65%
50mg
$ 828.00

ChemScene
TZ9 99.65%
10mg
$ 216.00

Cayman Chemical
TZ9 ≥98%
5mg
$ 122.00

Total 8 raw suppliers

Chemical Property of TZ-9

Chemical Property:

Boiling Point:675.9±65.0 °C(Predicted)
PKA:3.69±0.10(Predicted)
Density:1.477±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

SMI#9 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of TZ-9

There total 7 articles about TZ-9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 6-(bromomethyl)-N₂-phenyl-1,3,5-triazine-2,4-diamine

: 62-23-7
4-nitro-benzoic acid

: 1002789-86-7
(4-amino-6-(phenylamino)[1,3,5]triazin-2-yl)methyl 4-nitrobenzoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h; Reflux;
DOI:10.1016/j.tetlet.2014.10.122

Reference yield: 67.0%

: 99056-81-2
{4-amino-6-(phenylamino)-[1,3,5]triazin-2-yl}methanol

: 122-04-3
4-nitro-benzoyl chloride

: 1002789-86-7
(4-amino-6-(phenylamino)[1,3,5]triazin-2-yl)methyl 4-nitrobenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 40 ℃;
DOI:10.1016/j.tetlet.2014.10.122

Reference yield:

: 62-53-3
aniline

: 1002789-86-7
(4-amino-6-(phenylamino)[1,3,5]triazin-2-yl)methyl 4-nitrobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / water / 18 h / 90 °C

1.2: sodium alkoxide / 3 h / 20 °C

2.1: methanol / 16 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / Reflux

With hydrogenchloride; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tetlet.2014.10.122