dibenzhydryl N⁶,N⁶,O^2',O^7'-tetrabenzoylgriseolate

Base Information

• Chemical Name: dibenzhydryl N⁶,N⁶,O^2',O^7'-tetrabenzoylgriseolate
• CAS No.: 98871-11-5
• Molecular Formula: C₆₈H₄₉N₅O₁₂
• Molecular Weight: 1128.16
• Mol file: 98871-11-5.mol

Synonyms:

Chemical Property of dibenzhydryl N⁶,N⁶,O^2',O^7'-tetrabenzoylgriseolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibenzhydryl N⁶,N⁶,O^2',O^7'-tetrabenzoylgriseolate

There total 3 articles about dibenzhydryl N⁶,N⁶,O^2',O^7'-tetrabenzoylgriseolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

benzoyl chloride (98-88-4) + dibenzhydryl griseolate (98871-07-9) → dibenzhydryl N6,N6,O2',O7'-tetrabenzoylgriseolate (98871-11-5)

Guidance literature:

In pyridine; for 16h; Ambient temperature; ptotection from moisture;

DOI:10.1248/cpb.35.1036

Reference yield:

griseolic acid (79030-08-3,99146-56-2) → dibenzhydryl N6,N6,O2',O7'-tetrabenzoylgriseolate (98871-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 95.5 percent / acetone; H₂O / 16 h / Ambient temperature

2: 92.5 percent / pyridine / 16 h / Ambient temperature; ptotection from moisture

In pyridine; water; acetone;

DOI:10.1248/cpb.35.1036

Reference yield:

diazodiphenylmethane (908093-98-1) → dibenzhydryl N6,N6,O2',O7'-tetrabenzoylgriseolate (98871-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 95.5 percent / acetone; H₂O / 16 h / Ambient temperature

2: 92.5 percent / pyridine / 16 h / Ambient temperature; ptotection from moisture

In pyridine; water; acetone;

DOI:10.1248/cpb.35.1036

upstream raw materials:

benzoyl chloride

dibenzhydryl griseolate

griseolic acid

diazodiphenylmethane

Downstream raw materials:

N⁶-benzoylgriseolic acid

N⁶,O^2',O^7'-tribenzoylgriseolic acid, disodium salt

Refernces