(2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

Base Information

Chemical Name:(2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran
CAS No.:239437-74-2
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

(2RS,4R)-4-<N-(benzyloxycarbonyl)amino>-4-benzyl-2-hydroxy-5-oxotetrahydrofuran

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Chemical Property of (2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

Chemical Property:

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Technology Process of (2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

There total 3 articles about (2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131288-65-8
(2S)-N-(benzyloxycarbonyl)-2-allylphenylalanine

: 239437-74-2
(2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

Guidance literature:: With sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; ethyl acetate; for 24h;
DOI:10.1021/jm990140n

Reference yield:

: 95260-60-9
(2S,4S)-benzyl 4-benzyl-5-oxo-2-phenyloxazolidine-3-carboxylate

: 239437-74-2
(2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KN(TMS)2 / 1.) THF, toluene, 30 min, 2.) THF, toluene, a) -78 deg C, 3 h, b) from -78 deg C to RT, 4 h

2: 100 percent / 1 N aq.NAOH / methanol / 16 h / Heating

3: OsO₄, NaIO₄ / tetrahydrofuran; ethyl acetate / 24 h

With sodium hydroxide; sodium periodate; osmium(VIII) oxide; potassium hexamethylsilazane; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1021/jm990140n

Reference yield:

: 131288-31-8
(2S,4S)-2-phenyl-3-(benzyloxycarbonyl)-4-benzyl-4-allyloxazolidinone

: 239437-74-2
(2RS,4R)-4--4-benzyl-2-hydroxy-5-oxotetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 1 N aq.NAOH / methanol / 16 h / Heating

2: OsO₄, NaIO₄ / tetrahydrofuran; ethyl acetate / 24 h

With sodium hydroxide; sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1021/jm990140n