(1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

Base Information

Chemical Name:(1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane
CAS No.:211239-39-3
Molecular Formula:C₃₄H₄₃NO₈
Molecular Weight:593.717
Hs Code.:

(1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

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Chemical Property of (1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

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Technology Process of (1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

There total 1 articles about (1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid (2S,3S,4R,5S,6R)-5-benzyloxy-6-benzyloxymethyl-2-methoxy-4-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-ylamino)-tetrahydro-pyran-3-yl ester

: 211239-39-3
(1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 60 ℃; for 36h; Yield given;
DOI:10.1016/S0008-6215(98)00045-7

Reference yield:

: 211239-39-3
(1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

: 211237-50-2
(1S,2S,3R,6S)-6-((2S,3R,4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-methoxy-tetrahydro-pyran-3-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol

Guidance literature:: Multi-step reaction with 2 steps

2: 78 percent / Na, NH₃(l) / tetrahydrofuran / 15 h / -75 °C

With ammonia; sodium; In tetrahydrofuran;
DOI:10.1016/S0008-6215(98)00045-7

Reference yield:

: 127-09-3
sodium acetate

: 211239-39-3
(1R,2S,4R,5S,6S)-5-Benzyloxy-4-benzyloxymethyl-2-methoxy-7-((3aS,4S,9aR,9bS)-2,2,8,8-tetramethyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-3-oxa-7-aza-bicyclo[4.1.0]heptane

: Acetic acid (2S,3S,4R,5S,6R)-5-benzyloxy-6-benzyloxymethyl-2-methoxy-4-((1S,4R,5S,6S)-4,5,6-trihydroxy-3-hydroxymethyl-cyclohex-2-enylamino)-tetrahydro-pyran-3-yl ester

: Acetic acid (2R,3S,4R,5R,6S)-3-benzyloxy-2-benzyloxymethyl-6-methoxy-5-((1S,4R,5S,6S)-4,5,6-trihydroxy-3-hydroxymethyl-cyclohex-2-enylamino)-tetrahydro-pyran-4-yl ester

Guidance literature:: In water; acetic acid; at 90 ℃; for 72h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0008-6215(98)00045-7