C₁₅H₂₀O₄

Base Information

Chemical Name:C₁₅H₂₀O₄
CAS No.:1616872-87-7
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

C<sub>15</sub>H<sub>20</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀O₄

Chemical Property:

Purity/Quality:

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Pictogram(s):
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Technology Process of C₁₅H₂₀O₄

There total 2 articles about C₁₅H₂₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94235-22-0
(E)-2-methylbut-2-en-1-yl benzoate

: 1616872-87-7
C₁₅H₂₀O₄

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hexacyanoferrate(III); potassium carbonate; potassium osmate; hydroquinidein 1,4-phthalazinediyl diether; methanesulfonamide / dichloromethane; tert-butyl alcohol; water / 16 h / 0 °C

2: toluene-4-sulfonic acid / acetone / 0.5 h / Inert atmosphere

With potassium osmate; methanesulfonamide; potassium carbonate; toluene-4-sulfonic acid; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); In dichloromethane; water; acetone; tert-butyl alcohol; 1: |Sharpless Dihydroxylation;
DOI:10.1002/chem.201402254

Reference yield:

: C₁₂H₁₆O₄

: 77-76-9
2,2-dimethoxy-propane

: 1616872-87-7
C₁₅H₂₀O₄

Guidance literature:: With toluene-4-sulfonic acid; In acetone; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201402254

Reference yield:

: 1616872-87-7
C₁₅H₂₀O₄

: 1616873-17-6
C₂₅H₁₇ClO₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydroxide / methanol / 2 h / 20 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 4 h / Molecular sieve; Inert atmosphere

3.1: sodium hexamethyldisilazane / 0.17 h / 0 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

4.1: chloroamine-T / dichloromethane; water; ethanol / 12 h / 50 °C

5.1: boric acid; hydrogen / water; ethanol / 22 h / 760.05 Torr / Inert atmosphere

6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 20 h / 65 °C / Inert atmosphere

7.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere

8.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

9.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

9.2: 0.33 h

10.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

11.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

12.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

12.2: 1 h / 0 °C / Inert atmosphere

13.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

With hydrogenchloride; dmap; ammonium cerium (IV) nitrate; water; hydrogen; sodium acetate; chloroamine-T; boric acid; sodium hexamethyldisilazane; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1002/chem.201402254