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Technology Process of dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium

dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium

Base Information
  • Chemical Name:dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium
  • CAS No.:1011532-85-6
  • Molecular Formula:C26H26Cl2O2Ti
  • Molecular Weight:489.277
  • Hs Code.:
dichloridobis-1-(2-methoxyphenyl)-(η<sup>5</sup>-cyclopentadienyl)titanium

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Chemical Property of dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium
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Technology Process of dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium

There total 1 articles about dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.4%

Li<sup>(1+)</sup>*C<sub>5</sub>H<sub>4</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub><sup>(1-)</sup>=Li(C<sub>5</sub>H<sub>4</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)

Li(1+)*C5H4CH2C6H4OCH3(1-)=Li(C5H4CH2C6H4OCH3)

titanium tetrachloride
7550-45-0

titanium tetrachloride

dichloridobis-1-(2-methoxyphenyl)-(η<sup>5</sup>-cyclopentadienyl)titanium
1011532-85-6

dichloridobis-1-(2-methoxyphenyl)-(η5-cyclopentadienyl)titanium

Guidance literature:
In tetrahydrofuran; byproducts: LiCl; under N2 atm. soln. TiCl4 in THF was added to soln. lithum cyclopentadienide in THF and refluxed at 85°C for 16 h; soln. was cooled, solvent was removed in vacuo, residue was extd. with CHCl3, filtered through Celite and evapd. in vacuo; elem. anal.;
DOI:10.1016/j.jorganchem.2007.11.037
upstream raw materials:

titanium tetrachloride

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