Technology Process of Phenyl 2,3,6,3',6'-penta-O-benzyl-α-maltoside
There total 4 articles about Phenyl 2,3,6,3',6'-penta-O-benzyl-α-maltoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminium trichloride; dimethylamine borane; 4 A molecular sieve;
In
tetrahydrofuran;
for 48h;
Ambient temperature;
DOI:10.1016/0008-6215(93)84024-Z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 69 percent / (+)-10-camphorsulfonic acid / dimethylformamide / 5 h / 19.5 Torr
2: 1.) NaH / 1.) DMF, 2 h, 0 deg C, 2.) room temperature, overnight
3: 75 percent / BH3*NMe2, AlCl3, mol. sieves 4 Angstroem / tetrahydrofuran / 48 h / Ambient temperature; selective ring opening reaction; other di-O-benzylidene derivative of maltotriose; other reducing agents and procedures
With
aluminium trichloride; dimethylamine borane; 4 A molecular sieve; sodium hydride; (+)-10-camphorsulfonic acid;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(93)84024-Z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) NaH / 1.) DMF, 2 h, 0 deg C, 2.) room temperature, overnight
2: 75 percent / BH3*NMe2, AlCl3, mol. sieves 4 Angstroem / tetrahydrofuran / 48 h / Ambient temperature; selective ring opening reaction; other di-O-benzylidene derivative of maltotriose; other reducing agents and procedures
With
aluminium trichloride; dimethylamine borane; 4 A molecular sieve; sodium hydride;
In
tetrahydrofuran;
DOI:10.1016/0008-6215(93)84024-Z
