1-(3,4-dimethoxyphenyl)butane-1,3-dione

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)butane-1,3-dione
CAS No.:13298-49-2
Molecular Formula:C12H14O4
Molecular Weight:222.241
Hs Code.:
Mol file:13298-49-2.mol

Synonyms:m,p-Dimethoxybenzoylacetone;1-(3,4-Dimethoxy-phenyl)-butan-1,3-dion;1-(3,4-dimethoxyphenyl)-1,3-butanedione;1-(3,4-Dimethoxyphenyl)-butan-1,3-dion;1-(3,4-dimethoxyphenyl)-butan-1,3-dione;1-(3,4-dimethoxy-phenyl)-butane-1,3-dione;

Suppliers and Price of 1-(3,4-dimethoxyphenyl)butane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(3,4-dimethoxyphenyl)butane-1,3-dione
50mg
$ 130.00

Crysdot
1-(3,4-Dimethoxyphenyl)butane-1,3-dione 95+%
10g
$ 972.00

Crysdot
1-(3,4-Dimethoxyphenyl)butane-1,3-dione 95+%
5g
$ 748.00

Total 7 raw suppliers

Chemical Property of 1-(3,4-dimethoxyphenyl)butane-1,3-dione

Chemical Property:

Melting Point:71-72 °C
Boiling Point:347.5±27.0 °C(Predicted)
PKA:9.04±0.10(Predicted)
PSA：52.60000
Density:1.116±0.06 g/cm3(Predicted)
LogP:1.86560

Purity/Quality:

97% ^*data from raw suppliers

1-(3,4-dimethoxyphenyl)butane-1,3-dione ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(3,4-dimethoxyphenyl)butane-1,3-dione

There total 5 articles about 1-(3,4-dimethoxyphenyl)butane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 141-78-6
ethyl acetate

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 13298-49-2
1-(3,4-dimethoxyphenyl)butane-1,3-dione

Guidance literature:: With sodium amide; at 60 ℃;
DOI:10.1016/j.bmc.2017.02.048

Reference yield:

: C₁₄H₁₆O₅

: 13298-49-2
1-(3,4-dimethoxyphenyl)butane-1,3-dione

Guidance literature:: With hydrogenchloride; In water; at 80 ℃; for 1h;
DOI:10.1002/chem.201303872

Reference yield:

: 2859-78-1
4-Bromoveratrole

: 13298-49-2
1-(3,4-dimethoxyphenyl)butane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloro(1,5-cyclooctadiene)palladium(II); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; magnesium chloride; triethylamine / 1,4-dioxane / 80 °C / Glovebox; Inert atmosphere

1.2: 80 °C / Glovebox; Inert atmosphere

1.3: 18 h / 80 °C

2.1: hydrogenchloride / water / 1 h / 80 °C

With hydrogenchloride; dichloro(1,5-cyclooctadiene)palladium(II); triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; magnesium chloride; In 1,4-dioxane; water;
DOI:10.1002/chem.201303872