C₁₅H₁₇Cl₂NO₆

Base Information

Chemical Name:C₁₅H₁₇Cl₂NO₆
CAS No.:1370463-68-5
Molecular Formula:C₁₅H₁₇Cl₂NO₆
Molecular Weight:378.209
Hs Code.:

C<sub>15</sub>H<sub>17</sub>Cl<sub>2</sub>NO<sub>6</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₇Cl₂NO₆

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Technology Process of C₁₅H₁₇Cl₂NO₆

There total 2 articles about C₁₅H₁₇Cl₂NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370463-65-2
C₁₅H₁₅Cl₂NO₆

: C₁₅H₁₇Cl₂NO₆

: 1370463-68-5
C₁₅H₁₇Cl₂NO₆

Guidance literature:: With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; (1S,2R)-(+)-N,O-Bis(diphenylphosphino)-1,2-diphenyl-2-(N-methyl)aminoethanol; In methanol; acetone; at 20 ℃; for 42h; under 760.051 Torr; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

Reference yield:

: 1370463-62-9
N-chloroacyl-2-(diethoxyphosphoryl)glycinate

: C₁₅H₁₇Cl₂NO₆

: 1370463-68-5
C₁₅H₁₇Cl₂NO₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.02 h / 0 - 4 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; (1S,2R)-(+)-N,O-Bis(diphenylphosphino)-1,2-diphenyl-2-(N-methyl)aminoethanol / methanol; acetone / 42 h / 20 °C / 760.05 Torr / Inert atmosphere

With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; (1S,2R)-(+)-N,O-Bis(diphenylphosphino)-1,2-diphenyl-2-(N-methyl)aminoethanol; In methanol; dichloromethane; acetone; 1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;