Technology Process of C25H30N2O2S2
There total 12 articles about C25H30N2O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Lawessons reagent; pyridine / toluene / 100 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran
3: thionyl chloride / toluene
4: N-ethyl-N,N-diisopropylamine / acetonitrile
With
Lawessons reagent; pyridine; thionyl chloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 5 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
2: Lawessons reagent; pyridine / toluene / 100 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran
4: thionyl chloride / toluene
5: N-ethyl-N,N-diisopropylamine / acetonitrile
With
Lawessons reagent; pyridine; thionyl chloride; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 7 steps
1: PhMe2NBr3
2: sodium diformamide
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
4: Lawessons reagent; pyridine / toluene / 100 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran
6: thionyl chloride / toluene
7: N-ethyl-N,N-diisopropylamine / acetonitrile
With
Lawessons reagent; pyridine; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067