Phosphine oxide, (3-methyl-2-butenyl)diphenyl-

Base Information

Chemical Name:Phosphine oxide, (3-methyl-2-butenyl)diphenyl-
CAS No.:13303-61-2
Molecular Formula:C17H19OP
Molecular Weight:270.311
Hs Code.:

Synonyms:

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Chemical Property of Phosphine oxide, (3-methyl-2-butenyl)diphenyl-

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Technology Process of Phosphine oxide, (3-methyl-2-butenyl)diphenyl-

There total 14 articles about Phosphine oxide, (3-methyl-2-butenyl)diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 4145-83-9
(3-methylbuta-1,2-dien-1-yl)diphenylphosphine oxide

: 13303-61-2
3-methylbut-2-en-1-yl(diphenyl)phosphine oxide

Guidance literature:: With trichlorosilane; In benzene; at 80 ℃; for 24h; Reagent/catalyst; Solvent; Temperature; High pressure;
DOI:10.1134/S1070428017070065

Reference yield: 82.0%

: 870-63-3
prenyl bromide

: 791-28-6
Triphenylphosphine oxide

: 13303-61-2
3-methylbut-2-en-1-yl(diphenyl)phosphine oxide

Guidance literature:: Triphenylphosphine oxide; With sodium hydride; lithium iodide; In tetrahydrofuran; at 60 ℃; for 13h; Inert atmosphere;

prenyl bromide; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c8cc00289d