(3-Methylbut-2-en-1-yl)(diphenyl)phosphane

Base Information

Chemical Name:(3-Methylbut-2-en-1-yl)(diphenyl)phosphane
CAS No.:27387-44-6
Molecular Formula:C17H19P
Molecular Weight:254.312
Hs Code.:
DSSTox Substance ID:DTXSID50507211
Nikkaji Number:J1.979.041J

Synonyms:27387-44-6;(3-Methylbut-2-en-1-yl)(diphenyl)phosphane;DTXSID50507211

Suppliers and Price of (3-Methylbut-2-en-1-yl)(diphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of (3-Methylbut-2-en-1-yl)(diphenyl)phosphane

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:254.122437604
Heavy Atom Count:18
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCP(C1=CC=CC=C1)C2=CC=CC=C2)C

Technology Process of (3-Methylbut-2-en-1-yl)(diphenyl)phosphane

There total 7 articles about (3-Methylbut-2-en-1-yl)(diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 829-85-6
diphenylphosphane

: 78-79-5,9003-31-0
isoprene

: 27387-44-6
(3-methyl-2-butenyl)diphenylphosphine

Guidance literature:: With potassium hydroxide; In water; dimethyl sulfoxide; at 20 - 25 ℃; for 1h;

Reference yield:

: 829-85-6
diphenylphosphane

: 78-79-5,9003-31-0
isoprene

: 942202-30-4
C₁₇H₁₉P

: 27387-44-6
(3-methyl-2-butenyl)diphenylphosphine

Guidance literature:: With bis(trimethylsilyl)acetylenetitanocene; In toluene; at 90 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.200901863

Reference yield:

: 829-85-6
diphenylphosphane

: 27387-44-6
(3-methyl-2-butenyl)diphenylphosphine

Guidance literature:: diphenylphosphane; With n-butyllithium; In hexane; at 0 - 20 ℃; Inert atmosphere; Schlenk technique; Glovebox;

3,3-dimethylallyl halide; In hexane; at 0 - 20 ℃; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1021/acs.organomet.0c00144